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GCMS analysis results for sample AD28267, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD28267 conducted on November 30, 2001.

NYC-WTC_000034415–000034423

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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Scanned page image, NYC-WTC_000034422
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2601\28267.D vial: 25 Acq On : 27 Nov 2001 12:22 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.51 ug/1 98017 1,4-Dichlorobenzene-d4 11.70 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 35 3 Benzenamine, N-methyl-4-nitro- 152 C7H8N202 000100-15-2 14 4 2-Methyl-6-nitroaniline 152 C7H8N202 000570-24-1 10 Abundance 7 Scan 710 (11.559 min): 28267.D (-) m/z 149.90 100.00% 150

5000 115

52 78 38 63 I . 'ri''. I 1 87 . 11.20 11.40 11.60 11.80 ' ' — 'TH/ m/z 151.90 . 64.52% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 11.20 1.40 11,60 11.80 ' ' ' 52 78 m/z 114.90 37.23%

miz—> 20 30 35 40 50 ■ ■ i • • ....................... 1/ I " 1 11 " " I " 60 70 80 90 100 110 120 130 140 150 160 I— — Abundance #9592: Benzene-1 ,2,3,4-d4-, 5,6-dichloro- 150 ' i ' ‘ ' •i■ • ■ ' ■T 1 ' 1 ■ i■ 115 11.20 11,40 11,60 11.80 5000 52 78 m/z 78.05 . 16.20%

35 I_____ ■ ■ i ■ ■' ■ i ■ ■'' i m/z—> 20 30 40 50 Abundance • ■ I" • ■" I" ■ 60 70 87 1 __ . T’"E-T-TTIT-IIIT-7 + I'' '' I' ‘ 80 90 100 110 120 130 140 150 160 #10120: Benzenamine, N-methyl-4-nitro- 1— T 11 TT 152 11.20 11.40 11.60 11.80 m/z 52.00 14.80% 77 122 110 5000 65 30 94 . .............. 46........ • TTTT TT • ‘ i • ■ • < i ■ ■ ■ ■ i miz-s 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 1140 11.60 11.80 ’ ''

28267.D GCMS1126.M Fri Nov 30 13:11:07 2001 Page 1

NYC-WTC_000034422

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NYC-WTC_000034422Source: NYC Law Department, mirrored locally

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