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GCMS analysis results for sample AD28434, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD28434 conducted between November 21 and 26, 2001.

NYC-WTC_000034302–000034310

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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Scanned page image, NYC-WTC_000034309
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2901\28434.D vial: 26 Acq On : 29 Nov 2001 12:36 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************* * * ************************************ Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.57 0.50 ug/1 101706 1,4-Dichlorobenzene-d4 11.69 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 50 2 Benzene-1,2.3, 4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 16 3 Benzenamine, 2-methyl-4-nitro- 152 C7H8N202 000099-52-5 14 4 Benzenamine, 2-methyl-5-nitro- 152 C7H8N202 000099-55-8 10 Abundance Scan 710 (11.566 min): 28434.D (-) m/z 149.90 100.00% 150

5000 115 52 78 r | i-n i TTITuus . । i . k . । . 1120 11.40 11.60 11.80

mlz—> .... 30 +1 40 38 |, , 61 ■ -er 50 60 70 80 87 *TT — 90 100 110 120 I ' ' ' ' I 130 140 150 160 1— m/z 151.90 . 60.93% Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 78 11.20 11.40 11.60 11.80 52 m/z 114.90 . 36.11%

mlz-> 35 TI—TTTITTrIT 30 40 50 ' ■ i ■' '' i'' 60 70 80 87 11 11111" 111' TITI 4.1WPTTTPTTTT 90 100 110 120 130 140 150 160 L—— Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150

115 11.20 11.40 11.60 11.80 1 5000 52 78 m/z 78.05 . 18.91%

35 87 1 ■ ■ I ' 1 ' ' I ' ' ' ' I T-r-|-n-n-p-r i +1 ■ ■ ‘117111118 I 4— mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10129: Benzenamine, 2-methyl-4-nitro- ---------------------- 77 106 152 1120 11.40 11.60 11.80 m/z 52.00 15.28%

5000 51 94 66 ‘ * I * * « 1 I ' ' 1 ’ I — — TIT 1 1 1 1 T ' i ■ • ■ ■ i ■ ■ ■ ■ I ■ ■ ■ ■ i ■ ' ' 1 i ■ m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

28434.D GCMS1126.M Fri Nov 30 13:26:30 2001 Page 1

NYC-WTC_000034309

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NYC-WTC_000034309Source: NYC Law Department, mirrored locally

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