Laboratory report documenting GCMS analysis of sample AD28473 conducted between November 21 and 26, 2001.
NYC-WTC_000034258–000034270Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C: \HPCHEM\ 1 \DATA\NOV2 601\28473A.D vial: 5 Acq On : 27 NOV 2001 9:12 pm Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise t Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.52 ug/1 124680 1,4-Dichlorobenzene-d4 11.69 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1, 2,3, 4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 33 3 Benzenamine, 2-methyl-4-nitro- 152 C7H8N202 000099-52-5 22 4 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 14 Abundance Scan 710 (11.566 min): 28473A.D (-) m/z 149.90 100.00% 150
5000 115 52 78 ! 11.20 11.40 11.60 11.80 1 ‘ I mtm 48_L 4 38 62 207 TTTTTTTTT’II’TT q-m-r l I I M | II M |M H| I i BTT m/z 151.90 67.84% miz-> 30 50 GO 70 80 90 100110 120 130140 150 160 170 180 190 200 210 Abundance #9593:1,4-Dichlorobenzene-d4 150
5000 115 TT**T‘Tm‘TT 78 11.20 11.40 11.60 11.80 52 m/z 114.90 . 31.97% 35 87 - lm • 11 • *»• 11 ’I •"I ""I" TTTTIWTTTT mlz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Ab undance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150
115 11.20 11.40 11.60 11.80 5000 52 78 m/z 78.05 . 18.59%
35 87 I "II"TTTI"TTT 1 T-rq-rn-rpT i4 H ■ r u 11" " PTTTTT I................... -I- miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #10129: Benzenamine, 2-methyl-4-nitro- 1$2 TI T T T 77 106 11.20 11.40 11.60 11.80 m/z 52.00 16.01%
5000 51 94 66|
m/z—> MU ‘IT’ TTTpTTTp-rTTpTTTp-rrrp-rTTYm 30 40 50 60 70 80 90 100 110 120 130140 150 160 170 180 190 200 210 ' I ' ' ■ ’ I ' ' ' ' I 1 ' ■ • I ' 11.20 11.40 11.60 11.80
28473A.D GCMS1126.M Fri Nov 30 13:23:34 2001 Page 2
NYC-WTC_000034269
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NYC-WTC_000034289
Gas chromatography-mass spectrometry analysis of sample AD28432 conducted November 30, 2001, detecting other unknown compounds with results referenced in comments.
1 shared non-person entities · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034877
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28477 analyzed in early December 2001.
1 shared non-person entities · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034790
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28599 analyzed in early December 2001.
1 shared non-person entities · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034741
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28600 analyzed in early December 2001.
1 shared non-person entities · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034376
Laboratory commentary dated December 3, 2001, regarding sample AD28469 analysis, noting bis(2-Ethylhexyl)phthalate presence.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034415
Laboratory report documenting GCMS analysis of sample AD28267 conducted on November 30, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034750
Laboratory analyst notes on GCMS scan results detecting bis(2-ethylhexyl)phthalate and recovery rates for sample AD28594.
1 shared non-person entities · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034844
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28665 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034271
Laboratory report documenting GCMS analysis of sample AD28433 conducted on November 30, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034781
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28652 analyzed in early December 2001.
1 shared non-person entities · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034919
Laboratory report detailing GCMS scan results for sample AD28596, noting phthalate detection and recovery rates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034860
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28667 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000034154
Single page of raw GCMS data or header information from samples tested in late November 2001.
Filed in the same folder
NYC-WTC_000034155
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
Filed in the same folder
NYC-WTC_000034156
Instrument sequence log listing calibration standards and sample IDs processed between November 26 and 30, 2001.
Filed in the same folder
NYC-WTC_000034160
Laboratory report of a method blank analysis for sample AD28263 conducted on November 26, 2001.
Filed in the same folder
NYC-WTC_000034168
Laboratory report of GCMS calibration data for sample AD28263 conducted on November 26, 2001.
Filed in the same folder