Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
NYC-WTC_000034213–000034226Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2601\28271.D Vial: 26 Acq On : 27 Nov 2001 1:21 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 6 R.T . EstConc Area Relative to ISTD R.T. 11.56 0.51 ug/1 116256 1,4-Dichlorobenzene-d4 11.69
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,4 -Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1, 2,3,4-d4- , 5,6-dichloro- 150 C6C12D4 002199-69-1 17 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 14 4 2-Methyl-6/nitroaniline___________ 152 C7H8N202 _____ 000570-24-1 12 Abundance C Scan 710 (11.564 min): 28271.D (-) m/z 149.90 100.00% 150
5000 - 115 1 52 78 TT——————ur—DTTnv 1 rro3811 ■ THT 1,63 87 ,1______________ 207 + । — 1111111 — "*TT—IOI—C—UUI0-TTTg’TT mz—>30 40 50 60 7C 80 90 100 110 120 130 140 150 160 170 180 190 200 210 mmmmm 11 20 11.40 11,60 11.80 m/z 151.90 65.36% Abundance #9593:1,4-Dichlorobenzene-d4 I 150
50001 115 52 78 11'20 11.40 11.60 11.80 ' m/z 114.90 38.03% 87 4 .35. — Hmm . ... .. ...... — m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 • ■ I ' i 11 20 11.40 11.60 11.80 115 5000 52 78 m/z 78.05 . 20.64% I l i I — m — "i I "87: ■1111'''' I' 4 । >... 11.1 h , ।.... ।. — 11111 > n 11111 1— 35 1 mm TTTTTT DTTTT 5 1 m/z—>__ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 ......... _ Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- • I ‘ 1 ‘ ' I ' 1 ''l ’' TIBnm 152 11.20 11.40 11.60 11.80 m/z 52.00 . 15.85% 106 5000 | 53 81
92 122 m/z-> —. - . — .,, -m m 136 — — , । —. mm 11 20 1140 11.60 11.80 "d" 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210
28271.D GCMS1126.M Wed Dec 05 13:14:49 2001 Page 1
NYC-WTC_000034220
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NYC-WTC_000034402
Laboratory report documenting GCMS analysis of sample AD28428 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034808
Laboratory analyst notes on GCMS scan results, recovery rates, and low pH conditions for sample AD28649.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034886
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034198
Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033752
Analytical commentary for sample AD28159 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033834
Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000034154
Single page of raw GCMS data or header information from samples tested in late November 2001.
Filed in the same folder
NYC-WTC_000034155
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
Filed in the same folder
NYC-WTC_000034156
Instrument sequence log listing calibration standards and sample IDs processed between November 26 and 30, 2001.
Filed in the same folder
NYC-WTC_000034160
Laboratory report of a method blank analysis for sample AD28263 conducted on November 26, 2001.
Filed in the same folder
NYC-WTC_000034168
Laboratory report of GCMS calibration data for sample AD28263 conducted on November 26, 2001.
Filed in the same folder