GCMS analysis results for sample AD28468, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2901\28468.D Vial: 24 Acq On : 29 Nov 2001 10:39 am Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplrs 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************************* * * ************ Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.52 ug/1 117051 1,4-Dichlorobenzene-d4 11.70

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1, 2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 17 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 10 4 Acenaphthylene_________ _________________ 152 C12H8 000208-96-8 9 Abundance 7 Scan 710 (11.559 min): 28468.D (-) m/z 149.90 100.00% 150

5000 115

52 78 1120 11.40 11.60 11.80 38 mz-> ■ > 1 ■ 30 ,63 , ------ I —++ । - 40 50 60 87 70 80 90 100 110 120 —L 130 140 - 150 160 m/z 151.90 . 61.51% Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 "I 78 11.20 11.40 11.60 11.80 52 m/z 114.90 . 37.71% 87 tnfz~> 30 35 40 50 ■n-p-m-j-TT TBur 11—————— 60 70 80 90 100 110 120 130 +.... . 1 1 TT - 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150

11.20 11'40 11.60 11.80 115 5000 52 78 m/z 77.95 _ 19.37%

mfz~> Abundance 35 I ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ I ■ ■ ' ' I ' ■ 30 40 50 60 70 80 90 100 110 120 130 T‘8 87 , I ‘1‘t‘111TTIII" + 1— #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 140 150 160

152 n'20 1140 11.60 11.80 1 m/z 52.00 . 15.14% 106 5000 53 81

92 122 । ' ■ i ■' ■' i ■ ■'' i TI T |.... '1... 136.... L TT-p-T-rr-p-r m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 1140 11.60 11.80 '

28468.D GCMS1126.M Fri Nov 30 13:27:00 2001 Page 1

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