Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
NYC-WTC_000034331–000034346Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2901\28427.D Vial: 27 Acq On : 29 Nov 2001 1:35 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.51 ug/1 117029 1,4-Dichlorobenzene-d4 11.70 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 40 3 Benzaldehyde, 2-hydroxy-5-methoxy- 152 C8H803 000672-13-9 9 4 Benzoic acid, 2,3-dimethyl-______ 150 C9H10O2 000603-79-2 9 Abundance Scan 711 (11.568 min): 28427.D (-) m/z 149.90 100.00% 150
5000 115 78 52 11.20 11.40 11.60 11.80 38 45 | 63 1— ,,I'1l111.,1.. .... m/z 37I.... 103— _ ''111'1'1111 4...... 51.90 . 60.72% mlz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150
5000 115 52 78 11.20 11.40 11.60 11.80 1 m/z 115.00 , 35.88%
mlz-> 30 35 1 1 i ’ ' ' ■ I 1 1 1 • I 40 50 ■ ■ i ’ ■ ■ ' i ' ■ 87 111 — — -PP 111 60 70 80 90 100 110 120 130 1.1............. 140 I I——— 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150
115 1l'20 11.40 11.60 11.80 ' 5000 52 78 m/z 78705 21.94%
35 87 1 | i ■ • <»l1 < ■1 i > ■' > । ■ ■ J — ■ ■ r ■ ■' i ■ • mfz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66902: Benzaldehyde, 2-hydroxy-5-methoxy- T T TT 152 11.20 11.40 11.60 11.80 m/z 52.00 14.70% 137 5000 53 81 109 63 I 95 ' । | । । । • | ' ' ' 1 | Il i ' | Ji • ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ —... “I" i 11 ■ ■ TII ■ ■ ■ i ■ . ' I ' ' ' • i • ■ '~l • ' ■ ll ■ 1 ■ ‘ i ■ m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80
28427.D GCMS1126.M Fri Nov 30 13:25:09 2001 Page 1
NYC-WTC_000034338
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NYC-WTC_000034198
Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035700
Laboratory notes stating the GCMS scan of sample AD28901 revealed no unusual compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034213
Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034402
Laboratory report documenting GCMS analysis of sample AD28428 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033834
Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033752
Analytical commentary for sample AD28159 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000034154
Single page of raw GCMS data or header information from samples tested in late November 2001.
Filed in the same folder
NYC-WTC_000034155
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
Filed in the same folder
NYC-WTC_000034156
Instrument sequence log listing calibration standards and sample IDs processed between November 26 and 30, 2001.
Filed in the same folder
NYC-WTC_000034160
Laboratory report of a method blank analysis for sample AD28263 conducted on November 26, 2001.
Filed in the same folder
NYC-WTC_000034168
Laboratory report of GCMS calibration data for sample AD28263 conducted on November 26, 2001.
Filed in the same folder