Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
NYC-WTC_000033780–000033788Folder label: “GCMS X 11/20/01 A 11/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C: \HPCHEM\ 1 \DATA\NOV2 601\28149.D Vial: 15 Acq On : 27 Nov 2001 12:23 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.49 ug/1 110332 1,4-Dichlorobenzene-d4 11.69 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 64 2 Benzene-1,2,3,4-d4- , 5,6-dichloro- 150 C6C12D4 002199-69-1 43 3 Benzaldehyde/ 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 14 4 2-Methyl-6-nitroaniline 152 C7H8N202; 000570-24-1 12 Abundance Scan 709 (11.557 min): 28149.D (-) m/z 149.90 100.00% 150
5000 115
52 78 TI T T T 40 11.20 11.40 11.60 11.80 | 87 ’ O HH .66—++t । tr 11 TPTTT +1IPTITTTTT - a ■ — m/z 151.90 63.03% ti/z->_____ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150
5000 115 "T T T T 1120 11.40 11.60 11.80 52 78 m/z 114.90 37.34% 87 35 1 ' I 1 1 ' ' I ' • 1 1 I m/z->_____ 30 40 50 • • I' ' • ■ l • ■ 60 70 80 90 T —L 100 110 120 130 140 150 160 I 1 1 1 1 I
Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 ’TTr————u’’uu—rnr 115 11.20 11.40 11.60 11.80 5000 52 78 m/z 77.95 20.03%
35 87 ' 'I' ' ' U' 1 -PPPPPP IIPTTTTT '1 I 11 1' I' ' ‘ ■ I m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 — Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- TE T TT 152 1120 11.40 11.60 11.80 m/z 52.00 17.67% 106 5000 53 81
122 — 1 ' 1 — 92 ........ 1.......... 136........... ■ ' i ' ' 1 ' i ■ ' ' ' i " I' 1 " I " TT ■ i ■' I ■' ‘ * j i ‘ «J11 • ■ i • 1 1 ' f T’I0r m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80
28149.D GCMS1126.M Wed NOV 28 07:52:33 2001 Page 1
NYC-WTC_000033787
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NYC-WTC_000033825
Analytical commentary for sample AD28265 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033816
Analytical commentary for sample AD28325 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034249
Laboratory report documenting GCMS analysis of sample AD28277 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034384
Laboratory report documenting GCMS analysis of sample AD28429 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034393
Laboratory report documenting GCMS analysis of sample AD28470 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034366
Laboratory report documenting GCMS analysis of sample AD28468 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034302
Laboratory report documenting GCMS analysis of sample AD28434 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034415
Laboratory report documenting GCMS analysis of sample AD28267 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034271
Laboratory report documenting GCMS analysis of sample AD28433 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034852
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28668 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034860
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28667 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034844
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28665 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000033704
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000033705
Fragmented page from a GCMS-related record dated between November 20 and 26, 2001, likely part of the WTC environmental monitoring series.
Filed in the same folder
NYC-WTC_000033707
Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
Filed in the same folder
NYC-WTC_000033723
Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.
Filed in the same folder
NYC-WTC_000033726
Laboratory report of a GCMS reference analysis for sample AD28143 conducted on November 28, 2001, listing detected compounds and retention times.
Filed in the same folder