GCMS scan comments, Sample AD26133, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26133.D Vial: 59 Acq On : 30 NOV 2001 11:29 pm Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.63 ug/1 153274 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 14 4 2-Methyl-6-nitroaniline 152 C7H8N202 ____ 000570-24-1 12 Abundance Scan 710 (11.565 min): 26133.D (-) ? m/z 149.90 100.00% 150

5000 115 52 78 ...... -P PP — 11.20 11,40 11.60 11.80

mz—> • •i* 30 40 ■ - H4 A r 40 50 60 $4 70 87 -- — - 111 ■ ■ 80 90 100 110 120 130 140 150 160 m/z 151.90 60.56% Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 - 78 11.20 11.40 11.60 11.80 52 m/z 114.90 37.13%

miz-> Abundance 35 ' 30" "40' " '5b' •11 “ • • 11 ■ 87 1 1..»* । •.. i j... 11 i. 60 70 80 90 100 110 120 130 140 150 160 +- #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 TTTLOTumT 115 11.20 11.40 11.60 11.80 5000 52 78 m/z 78.05 20.39%

35 87 1 1 ■ i ■ ■ ■11 ■ ■1 ■ i TT-p-m-p-r J...... , +IPPPTTIT 1 I * ‘ ' 1 I i 1 i ► | i I : » | » i mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- - 152 11.20 11.40 11.60 11.80 m/z52.00 15.70% 106 5000 53 81

92 122 ■ ' i 1 ■ ' ■ i ■ ■ '1 i ■n-p-m-p-T 118 TIPPT - 11 ‘ 136 ‘1 * I * 1411 1’111 —————— m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

26133.D NP112601.M Mon Dec 03 10:07:15 2001 Page 3

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