GCMS analysis results for sample AD26080, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26080.D Vial: 58 Acq On : 30 NOV 2001 10:31 pm Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.57 ug/1 124641 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentati ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 64 2 Benzene-1,2,3.4- d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 23 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 10 4 4-Amino-2-chlorobenzonitrile 152 C7H5C1N2 ____ 020925-27-3 9 Abundance Scan 710 (11.559 min): 26080.b (-) 7 m/z 149.90 100.00% 150

5000 115 52 78 40 11.20 11.40 11.60 11.80 TTr — .. +A -mmmmmp 1 87 m/z 151.90 I 66.44% ■ ■ i ■ • • i ‘ ■ n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 IIn T II1—nn , . TIT 78 1120 11.40 11.60 11.80 52 m/z 115.00 39.24%

miz-> 35 ———nnnt 30 40 50 ■ i1 ■'11 ■ 87 i ■ ■ ■ ‘ i' i • • * * i 60 70 80 90 100 110 120 130 140 150 160 i *k ‘ i I—— Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- .. ............. ............................... 150 ‘ I ' ‘ ‘ ‘ I ‘ ‘ I * • * * I ‘ 1 * * I ‘

115 _ 11-20 11.40 11.60 11.80 5000 52 78 m/z 78.05 23.09%

35 87 - — ■ i ■ • ■ ■ i' T 111 i ■ • • ■ i • * I • • miz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 11/1/11/1/1-T ’——nO—OTGTT-T 152 11.20 11.40 11.60 11.80 m/z 52.00 17.38% 106 5000 53 81

i | i i ii । i i — . X I _ _ 92 ...... .122 । I 11 ■ ‘ ‘ ■ i ■ । ‘ • i ' i' ■ ■11 ‘ TT It ‘ * Ik ‘ m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

26080.D NP112601.M Mon Dec 03 09:41:09 2001 Page 2

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