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GCMS analysis results for sample AD26208, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26208 with unidentified compounds detected.

NYC-WTC_000031198–000031208

Folder label: “GCMS X 11/2/01 A 12/1/01

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Scanned page image, NYC-WTC_000031207
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26251.D Vial: 57 Acq On : 30 NOV 2001 9:32 pm Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.55 ug/1 119618 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene -1, 2/3, 4- d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 38 3 Benzalde!hyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 10 4 Benzofur Abundance 2 an, 7-chloro- 152 C8H5C10 024410-55-7 9 Scan 710 (11,560 min): 26251. D (-) m/z 149.90 100.00%| 150

5000 115

52 78 — 0 —— 40 87 11.20 11.40 11.60 11.80 — — .■.•. ] 11 #. — 66.41 — 1pr l 1 ( | > 1 1 1 | ! > m/z 151.90 67.29% mfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 52 78 11.20 11.40 11.60 11.80 ' m/z 114.90 39.17%|

miz-> 30 35 ' ' i ■ 1 1 11 • ‘ ‘ 11 40 50 ''' I'' ‘' I' ‘ 60 70 87 । • • • > । • • i ‘! 111 < | > i 80 90 - 100 110 120 130 140 150 160 L—— Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 I ' ‘ ‘ ‘ i 1 ' i ' ' ' • i 1 ■ ' ' i ' 115 1120 11.40 11.60 11.80 5000 52 78 m/z 78.05 20.51%

35 87

miz-> 30 I ‘ ‘ l ' ‘ ' I ' ‘ 40 ‘ I ' ‘ I ‘ ‘ ‘ ‘ I' ‘ _..................... i'. i.... t.... i.» ' i11 ‘ ' i ' ‘ ‘ ' i'1 i • ‘ 50 60 70 80 90 100 110 120 130 140 150 160 I——— Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- TTm/nt TTT । TTT > • i > 152 11.20 11.40 11.60 11.80 m/z 52.00 15.85% 106 5000- 53 81

122 r‘i••‘*I’‘ •I ■ ' I 11 ■' I 1 ‘ ‘I‘ TIP 92 — 136 JI TIITTI-171t18 •11 • • ‘ i ■ ' ' ■ i ■ ■ TTT । । , miz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

26251.D NP112601.M Mon Dec 03 09:43:26 2001 Page 2

NYC-WTC_000031207

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NYC-WTC_000031207Source: NYC Law Department, mirrored locally

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