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GCMS analysis results for sample AD26208, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26208 with unidentified compounds detected.

NYC-WTC_000031198–000031208

Folder label: “GCMS X 11/2/01 A 12/1/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\l\DATA\NOV3001\26251.D Vial: 57 Acq On 30 Nov 2001 9:32 pm Operator: 209 GALOS Sample 11/2 gc/ms Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.68 2.86 ug/1 626165 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone 4 -hydroxy-4-methyl- 116 C6H12O2 000123-42-2 83 2 Acetic acid , 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 Acetone 58 C3H60 000067-64-1 12 4 CH2=CHZH2C(O)OCH3___________________ 100 C5H802 003724-55-8 10 Abundance Scan 287 (7.677 min): 26251 .D (-) m/z 42.95 100.00% 43

5000 59 101 —PP 1PF I । i 7.40 7.60 7.80 8.00 7183 -mmtt . I.... I111... I.In|..111.... 11p,.11.... 1.... 1.1111u111 207 m/z 59.05 39.60% mlz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 Bmun—ammgvvr 59 7.40 7.60 7.80 8.00 m/z 58.05 18.90%

mz-> 27 ......... 11 । ""i ""i1 H . 101 .............................................. ..... . I’TUTITTTTTEET I • ।1।• 111.1 j • 1111 • • n p > । •! 11.111 r.. 11 > j 1111111

10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #3292: Acetic acid, 1,1-dimethylethyl ester 43 - —P* T I i 7.40 7.60 7.80 8.00 5000 57 m/z 100.95 15.25% 101 15 27 nmppmttt 11 TTIemTggj m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #62326: Acetone 1 • ■ ■ i ■ ■ 1 ■ i ■ 1 ■ ■ i TTTTr i . . . 43 7.40 7.60 7.80 8.00 m/z 41.05 5.78% 5000 58 27 ------- j >: H | i. ».j.H.।i.ii| l. . > Mii,t ».11.iM।.» .» , ’ i i | ! I i i।ilt >1111111111 ।: i i i • ' i ' ■ ' ■ i ■ ■ • • i ■ • • ' i ‘ m/z—> 10 2030405060 70 8090 100110120130140 150 160 170180 190200210 7.40 7.60 7.80 8.00

26251.D NP112601.M Mon Dec 03 09:43:24 2001 Page 1

NYC-WTC_000031206

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NYC-WTC_000031206Source: NYC Law Department, mirrored locally

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