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GCMS analysis results for sample AD25663, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD25663 conducted on November 29, 2001, noting other unknown compounds.

NYC-WTC_000069832–000069841

Folder label: “GCMS Scan X 10/26/01 An 11/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1601\25663.D Vial: 27 Acq On : 17 Nov 2001 4:25 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.83 ug/1 308662 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanon^ 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 72 2 Acetic aci/C 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 28 3 Acetone / 58 C3H6O 000067-64-1 12 4 3-Hydroxy-2-pentanone____________ 102 C5H10O2 003142-66-3 9 Abundance Scan 288 (7.687 min): 25663.D (-) m/z 43.00 100.00% 43

5000 59

101 ,,,, 83 , 7.40 7.60 7.80 8.00 207 I'' " I" " I' I " ' 11'"' I" " I''" I" " I " l""l ' ‘" I' m/z 59705 47713% mfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #64274: 2-Pentanone, 4-hydroxy-4-niethyl- 43

5000 . . . I . . I , I ,, I , TTVyr i , , 59 7.40 7.60 7.80 8.00 m/z 101.05 22.65% 27 101 I I .... ........... I.... I" " I" " I' ........ I n " I " "I p"I ■nfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #3292: Acetic acid. 1,1 -dimethylethyl ester 43

7.40 7.60 7.80 8.00 5000 57 m/z 58.05 19707% 101 ’ll® 2/ ""I""I I" " I" " r "' 1" " I ymTjrTTTyrTTTpTTTJT^^ TTfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #62326: Acetone 43 7.40 7.60 7.80 8.00 m/z 41.05 7.49% 5000 58 27 ... I'''.. 'I' 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 7.40 7.60 7.80 8.00

25663.D NP103001.M Wed Nov 28 14:19:36 2001 Page 1

NYC-WTC_000069840

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NYC-WTC_000069840Source: NYC Law Department, mirrored locally

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