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GCMS comments for sample AD28649, Dec 2001

Machine-extracted title · confidence 100%

Laboratory analyst notes on GCMS scan results, recovery rates, and low pH conditions for sample AD28649.

NYC-WTC_000034808–000034818

Folder label: “GCMS X 11/23/01 A 11/29/01

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Scanned page image, NYC-WTC_000034814
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2901\28593.D Vial: 36 Acq On : 29 Nov 2001 9:24 pm Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.50 ug/1 112871 l,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 003855-82-1 59 150 C6C12D4 2 Benzene-1,3,4-d4-, 5,6-dichloro- 002199-69-1 40 150 C6C12D4 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 38 4 Benzofuran, 7-chloro- ____________ 152 C8H5C10 ____ 024410-55-7 10 Abundance C Scan 710 (11.559 min): 28593.D (-) m/z 149.85 100.00% 150

5000 115 ■ i ■ ■ ' ' i ' ■ - PPP 52 78

m/z-> ......... .. 30 40 50 60 70 80 sz90 I ■ ■ ' ■ I 1 i 100 110 120 130 140 150 160 1120 11.40 11.60 11.80 m/z 151.90 . 68.73% Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 78 11.20 11.40 11,60 11.80 52 m/z 114.95 35.08% 35 87 - '' 111 ' ’ I' ■' * i ■ I'1 b 1 I 1 i ■''' i ■ ■ ■ ■ i ■' ■ ■ i ■ ■ mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 —>TT—————TTnT 115 1120 11,40 11,60 11.80 5000 52 78 m/z 52.00 19.07%

35 87 - —............. " 1 I " " I " I ' TTT1 1111 111 1 111 11 I. ।.... 11111111 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 152 11.20 11.40 11.60 11.80 '' m/z 78.00 . 17.96% 106 5000 53 81

- 92 122 । TPP |11..... 1...... 136....... 1, 1 ' i ' ' '' i 1 ' 1 1 i ■ ■ ■ ■ i 1 1 ■ ■ i ' ‘ 1 ■ I 1 1 1 1 P T TT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

28593.D GCMS1126.M Fri Nov 30 16:18:53 2001 Page 1

NYC-WTC_000034814

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NYC-WTC_000034814Source: NYC Law Department, mirrored locally

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