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GCMS analysis results for sample AD26128, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26128 conducted on December 3, 2001.

NYC-WTC_000030980–000030991

Folder label: “GCMS X 11/2/01 A 12/1/01

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Scanned page image, NYC-WTC_000030990
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26128.D Vial: 65 Acq On : 1 Dec 2001 5:21 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 11.56 0.58 ug/1 116765 1,4-Dichlorobenzene-d4 11.70 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 96 2 Benzene-1,2/3, 4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 59 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 27 4 Acenaphthylene__________________________ 152 C12H8 000208-96-8 10 Abundance Scan 710 (11.564 min): 26128. D (-) m/z 149.90 100.00% 150

5000 115 78 ----------------- 52

1 ‘ I ‘ , +2—1 — — — I I— m/z 151.90 38 45 40 50 60 87

70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 65.34% mz-> 30 Abundance #9593: 1,4-Dichlorobenzene-d4 KO

5000 115 TIU—OTTUp 78 11.20 11.40 11.60 11.80 52 m/z 115.00 39.18% 35 87 ■ ■ i. > i. 111111 I ' ' i •' 1 ‘ i ' ' i ■ • ■ ■ i11 ■ ■ I ■ ■ ■' I' ■ miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1 ,2,3,4-d4-, 5,6-dichloro- 1(0 — —PPI -P i — TI 115 11.20 11.40 11.60 11.80 m/z78.05 28.00% _____

I 5000 52 78

35 87 — — I——— _X ' ' I * '1 ' I' 1 m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 152 11.20 11.40 11.60 11.80 m/z 52.00 _ 22.70% 106 5000 53 81

122 • •| H * • ’ •l ’ ’ I ‘ ‘ ‘ I 92 mt ’It ■II1... 1 136 1 1117 ■ i1 • ■ ' i 1 ' ' ■ i TT , TTII , TTTT T 1 1 I1 m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

26128.D NP112601.M Mon Dec 03 12:15:59 2001 Page 3

NYC-WTC_000030990

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NYC-WTC_000030990Source: NYC Law Department, mirrored locally

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