GCMS analysis results for sample AD28277, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2601\28277 .D Vial: 28 Acq On : 27 Nov 2001 3:19 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.54 ug/1 118289 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 72 2 Benzene-1,2,3,4-d4- , 5,6 - dichloro - 150 C6C12D4 002199-69-1 45 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 25 4 Biphenylene 152 C12H8 000259-79-0 9 Abundance Scan 710 (11.558 min): 28277.D (-) m/z 149.90 100.00% 150

5000- 115 52 78 —‘1‘1——1——n—r—enu—Tr 1120 11.40 11.60 11.80 ' H A -++s3.4l 1— 87 ■ ■ । 38 44 TITT +l m/z 151.90 60.25% mlz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593: 1,4-Dichlorobenzene-d4 150

5000 115 T1——mmTTTTT 78 11.20 11.40 11.60 11.80 52 m/z 115.00 . 37.02%

mlz-> 35 TTf-rrnj-rrIIT 30 40 50 ■ ■ । ■ • • • । 60 70 • 80 ...... 1.1..... 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150

115 1120 11.40 11.60 11.80 5000- 52 78 m/z 52.00 . 19.11%

nfz~> 35 1111 — TPPT 30 40 50 • ■ । 60 ■ i ■ ■ 70 87 |______ , 1- — i ■ ■ • ■ i ■ ■ ■ ■ i ■ ■ ' ■ i ■ '

80 90 100 110 120 130 140 150 160 + — Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 152 11.20 11.40 11.60 11.80 111 ' m/z 78.05 . 19.03% 106 5000 53 81

— 92 -122 T’T n-n-p-m-j 136 | '11111'' l.— 1 i ' ■' • i' •'' i ■ ‘ i ■ ■ mfz~> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 1120 1140 11.60 11.80 1

28277.D GCMS1126.M Fri NOV 30 13:22:54 2001 Page 1

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