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GCMS analysis results for sample AD26207, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report identifying multiple organic compounds including 1,1'-oxybis(2-ethoxy-)ethane in sample AD26207.

NYC-WTC_000031187–000031197

Folder label: “GCMS X 11/2/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26208.D Vial: 55 Acq On : 30 Nov 2001 7:36 pm Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.56 ug/1 121096 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 72 2 Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Acenaphthylene 152 C12H8 000208-96-8 14 4 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 10 Abundance Scan 711 (11.569 min): 26208.D (-) m/z 149.90 ,100.00% 150

5000 115 78 ----- 52

m/z-> 38 — . ., 62 .I 87 m l— 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 ____________ 207 "I0——0———1—00—309T 1120 11.40 11.60 11.80 m/z 151.90 64.57% Abundance #9593:1,4-Dichlorobenzene-d4 1$0

5000 115 78 11.20 1140 11.60 11.80 ‘ ‘ ‘ ' 52 m/z 114.90 39.91% 35 87 " i ■■i‘1 ■11 ” ■ i'”' i “ TOTa■I'. I I . ■ I j ■ l . > l . I > 1 । 'I . . । , i । ■ । i . . । । . i , . । . . . . । . . . . । , . . mlz-> 30 40 50 60 70 80 90 100 110120 130140 150160 170 180 190 200 210 Abundance #9592: Benzene-1,2,3,4-84-, 5,6-dichIoro- 1$0 "I T 11 115 1120 11.40 11.60 11.80 5000 52 78 m/z 77.95 23.38%

35 87 | mmmm 111’011111711 "■l-" •l*■ HpTTUTT N11111.11.11.11.. 11. ।।. 111 >., miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #67013: Acenaphthylene 5 I 11I T, I I TII I J I I ] I I I I I I 1$2 11.20 11.40 11.60 11.80 m/z 52.00 17.21% 5000

76 63 126 i 87 98 । 11—001011011111 TIppmayumum TpmnOnpTDur mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 11.20 11.40 11.60 11.80

26208.D NP112601.M Mon Dec 03 09:42:47 2001 Page 2

NYC-WTC_000031196

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NYC-WTC_000031196Source: NYC Law Department, mirrored locally

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