GCMS comments for sample AD28155, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV2601\28155.D Vial: 11 Acq On : 26 Nov 2001 8:29 pm Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

11.56 0.49 ug/1 115349 1,4-Dichlorobenzene-d4 11.69

Hit# of Tentative ID MW MolForm CAS# Qual

1 1,4-Di hlorobenzene - d4 150 C6C12D4 003855-82-1 58 2 Benz ne-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 38 3 Acen phthylene 152 C12H8 000208-96-8 14 4 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 9 Abundance Scan 710 (11.565 min). 28155.D (-) m/z 149.90 100.00% 150

5000 115 78 "T TT 52 87 1 11.20 11.40 11.60 11.80 38 45 , . . <62 ■ ’ i1 ' ' + — I'1 1 H I — I ' TT .... 1 .... I 1 . I .... 1 .... 1 . 1— m/z 151.90 65.43% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593: 1,4-Dichlorobenzene-d4 150

_) 5000 115 ‘T T‘1 TT 11.20 11.40 11.60 11.80 52 78 m/z 115.00 36.69% 35 ■1 i ' 1 — 87— , L - miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1 ,2,3,4-d4-, 5,6-dichloro- 150 ‘I ...... 115 11.20 11.40 11.60 11.80 5000 52 78 m/z 78.05 20.59%

mlz-> 35 I______ ■ ' i ■ ■ ' ' i ■ ' ■ ■ i

30 40 50 ■ ■ । • • • ■ । 60 70 ■ 87 — 80 90 L I——— 100 110 120 130 140 150 160 Abundance #67013: Acenaphthylene TT T I’ 1$2 11.20 11.40 11.60 11.80 m/z 52.00 . 15.25% 5000

76 63 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ • ' I ■ i ■ ■1 ' i L■ 87 98.... 126 1 —Ig—t ‘I T Ti" m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

28155.D GCMS1126.M Tue Nov 27 12:58:11 2001 Page 1

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