GCMS analysis results for sample AD28431, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2901\28431.D Vial: 25 Acq On : 29 Nov 2001 11:38 am Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************************* ********** * * * * Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.53 ug/1 122651 1,4-Dichlorobenzene-d4 11.69 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2,3,4-d4-, 5,6-dichloro­ 150 C6C12D4 002199-69-1 16 3 Acenaphthy1ene 152 C12H8 000208-96-8 9 4 Biphenylene 152 C12H8 000259-79-0 9 Abundance Scan 710 (11.565 min): 28431 .D (-) m/z 149.90 ,100.00% 150

5000 115

52 78 ..... ................................ . 11.20 11.40 11.60 11.80 I 3845 63 — m/z 151.90 68. 33% T‘0‘THHtr I""I TI‘ mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150

______ _________ ___________ 5000 115 78 11.20 11.40 11.60 11.80 1 52 m/z 114.90 . 38.18% 87 35 1 ‘ I 1 1 ‘ ’ I 1 1 ’ 1 I •»i • ■ ■ • I' ■ i' ■ ’ ■ i ■ ■ ■ ■ i ■ ■ • ■ i ■' .1...... 1 1— miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1(0

115 11.20 11'40 11.60 11.80 1 5000 52 78 m/z 78.05 , 19.66%

mz-> Abundance 30 35 । • ■ । • ■ ■ ■ । ■ • ■ • । 40 50 ' ■ i ■ ■ ■' I •1 60 87 I i'1 ■' i'''' i ■ ■' ■ i ■' 70 80 90 100 110 120 130 #67015: Acenaphthylene + 140 47 150 160 mF 152 1120 11.40 11.60 11.80 m/z 52.00 . 16.01% 5000

76 63 126 87 98 — — —P 11 TTTT i TT, ' i ■ ’ ■ • i TIII m/z—> 30 40 50 60 70 80 90 100 11 120 130 140 150 160 11.20 1140 11.60 11.80 '

28431.D GCMS1126.M Fri Nov 30 13:26:00 2001 Page 1

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