GCMS analysis results for sample AD28429, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2701\28429.D vial: 21 Acq On : 28 Nov 2001 2:46 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.51 ug/1 110300 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 52 2 Benzene-1,2, 3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 28 3 Acenaphthylene 152 C12H8 000208-96-8 10 4 JP 60 / 151 C10H17N 013074-39-0 9 Abundance Scan 711 (11.569 min): 28429.D (-) m/z 149.90100.00% 150

5000

m/z-> Abundance 30 ■ ■ i ■ 52 .44 TTt1 ■ 1’87 I " ' ........... 40 50 60 70 80 78

90 100 110 120 130 #9593:1,4-Dichlorobenzene-d4 115

— 140 .1 11.20 11.40 11.60 11.80 I———60 m/z 151.90 150 61.86% ' ' I ’

150

5000 115 78 11 20 11.40 11.60 11.80 52 m/z 114.90 . 35.28% 87 35 1 111 ■111111 ' I PPIPTTITTT 'I............ . - mlz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 ------- 115 1120 11.40 11.60 11.80 5000 52 78 m/z 78.05 . 18.41%

35 87

mlz-> ‘‘ I 1′1411′1111 30 40 50 ■ ■ I' ' ' ' I ' ' 60 70 [ TTtETTTFITIT 80 90 ■ I ■ ' ■' I ■' ■' I' ' 100 110 120 130 140 150 160 Hu, Abundance #67013: Acenaphthylene ■ i ■ ■ ■ ■ i ■ • ■ 1 I ■ ■ ‘ • i ■ ■ 1 ■ i ' 1(2 1120 11.40 11.60 11.80 m/z 52.00 15.96% 5000

76 63 87 98 126 ■n । । T‘ 11‘‘111"‘i ‘111T TT‘trt—uu‘—IT-u——I—TO3I—IITIr +TTTT- m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 1140 11.60 11.80 1

28429.D GCMS1126.M Fri Nov 30 13:43:18 2001 Page 1

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