Laboratory commentary dated December 3, 2001, regarding sample AD28469 analysis, noting bis(2-Ethylhexyl)phthalate presence.
NYC-WTC_000034376–000034383Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C: \HPCHEM\ 1 \DATA\NOV2 901\28469.D Vial: 31 Acq On : 29 Nov 2001 3:32 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.51 ug/1 102259 1,4-Dichlorobenzene-d4 11.70
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2,,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 27 3 Benzofuran, 7-chloro- 152 C8H5C10 024410-55-7 9 4 JP 60 / 151 C10H17N 013074-39-0 9 Abundance Scan 711 (11.569 min): 28469.D (-) m/z 149.90 ,100.00% 150
5000 115 52 78 11.20 11.40 11.60 11.80
miz—> 30 IT 38 40 ..4 3. 4 50 60 87 ‘T‘11‘1‘7 T T‘T‘ 11 TTTT I 11............ 70 80 90 100 110 120 130 140 150 160 m/z 151.90 63.66% Abundance #9593:1,4-Dichlorobenzene-d4 150
5000 115 T ( , , , , ( , , , —| . . . . । l ,. < . । . 78 11.20 11,40 11,60 11.80 52 m/z 115.00 , 36”. 93% 87 mz—> 35 1' 11 1 11 1111' I 1 ' i' ' ' ■ i ' ' PPPT 30 40 50 60 70 80 90 100 110 120 130 L........ 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-,5,6-dichloro- 150
115 11.20 1l'40 11.60 11.80 ' 5000 52 78 m/z 78.05 19.31%
mlz-> Abundance 30 35 t 40 50 1 1'1111'1 60 70 87 —...................... + ■ ■ । • > ■ > । ■ 80 90 100 110 120 130 140 150 160 LI—— #10136: Benzofuran, 7-chloro- 152 11.20 11.40 11.60 11.80 m/z 52.00 15.27% 5000 89
63 35 49 73 125 ■ H 1 ' 1 I 1 1 1 1 i b 1 l ' - -1PP2 m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80
28469.D GCMS1126.M Fri Nov 30 13:15:38 2001 Page 1
NYC-WTC_000034382
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NYC-WTC_000034919
Laboratory report detailing GCMS scan results for sample AD28596, noting phthalate detection and recovery rates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034860
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28667 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034844
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28665 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034852
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28668 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034799
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28593 analyzed in early December 2001.
1 shared non-person entities · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034415
Laboratory report documenting GCMS analysis of sample AD28267 conducted on November 30, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034741
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28600 analyzed in early December 2001.
1 shared non-person entities · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034781
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28652 analyzed in early December 2001.
1 shared non-person entities · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034750
Laboratory analyst notes on GCMS scan results detecting bis(2-ethylhexyl)phthalate and recovery rates for sample AD28594.
1 shared non-person entities · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034877
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28477 analyzed in early December 2001.
1 shared non-person entities · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034868
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28597 analyzed in early December 2001.
1 shared non-person entities · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034790
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28599 analyzed in early December 2001.
1 shared non-person entities · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000034154
Single page of raw GCMS data or header information from samples tested in late November 2001.
Filed in the same folder
NYC-WTC_000034155
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
Filed in the same folder
NYC-WTC_000034156
Instrument sequence log listing calibration standards and sample IDs processed between November 26 and 30, 2001.
Filed in the same folder
NYC-WTC_000034160
Laboratory report of a method blank analysis for sample AD28263 conducted on November 26, 2001.
Filed in the same folder
NYC-WTC_000034168
Laboratory report of GCMS calibration data for sample AD28263 conducted on November 26, 2001.
Filed in the same folder