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GCMS analysis results for sample AD26080, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26080 conducted on December 3, 2001.

NYC-WTC_000030944–000030954

Folder label: “GCMS SCAN X 11/2/01 AN 11/30/01

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Scanned page image, NYC-WTC_000030952
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26080.D Vial: 58 Acq On : 30 Nov 2001 10:31 pm Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.68 2.99 ug/1 652959 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone ,/4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 Acetone / 58 C3H60 000067-64-1 16 3 Formamide/ N,N-diethyl- 101 C5H11NO 000617-84-5 9 4 Propanal, 2-hydroxy-2-methyl - 88 C4H802 020818-81-9 9 Abundance Scan 288 (7.685 min): 26080.D (-) m/z 42.95 100.00% 43

5000 59 — T— — = 1 — »

101 |_____________________________ 207 83 7.40 7.60 7.80 8.00 miz—> 0-mmmmm +97 TTTggg] 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190200210 m/ z 59.05 38.69% Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 ' 1 1 1 ‘n i j i I IIT i | rrrr 59 7.40 7.60 7.80 .00 m/z 58.05 21.84% 15 31 . 101

m/z-> mmmt TTTTggO83 .1 —gp]u 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190200210 Abundance #62322: Acetone 43 1 Tr1 1 1 1 ' 1 1 ' I 7.40 7.60 7.80 8.00 5000 m/z 100.95 15.92% 58 27

m/z-> mlmd Tpo TrTT 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190200210 Abundance #1629: Formamide, N,N-diethyl- ‘--111511 14/1.7 1 1TT11nuun 30 7.40 7.60 7.80 8.00 58 m/z 41.00 6.54% 101 5000- 44 86 72

miz—> TTTTT wp l T TTTTgg TTTTTprn-r 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 T.1111—1TT-r-r111′111" 7.40 7.60 7.80 8.00

26080.D NP112601.M Mon Dec 03 09:41:06 2001 Page 1

NYC-WTC_000030952

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NYC-WTC_000030952Source: NYC Law Department, mirrored locally

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