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GCMS analysis report, Sample AD26163, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26163 for unknown compounds conducted on December 3, 2001.

NYC-WTC_000031039–000031048

Folder label: “GCMS X 11/2/01 A 12/1/01

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Scanned page image, NYC-WTC_000031046
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3001\26163 .D Vial: 60 Acq On 1 Dec 2001 12:28 am Operator: 209 GALOS Sample 11/2 gc/ms Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.40 ug/1 304194 1,4-Dichlorobenzene-d4 11.70 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 78 2 Propanal,2-hydroxy-2-methyl- 88 C4H802 020818-81-9 25 3 Acetone 58 C3H60 000067-64-1 16 4 5-Hexen-2-one 98 C6H10O 000109-49-9 9 Abundance Scan 288 (7.687 min): 26163.D (-) 1 42.95 100.00% 43

5000 59

101 7,40 7.60 7.80 8.00

miz—> 10 mmmp 20 30 40 83 ! p 69 TTTTHTTTT ■p-n-rp T—U—"0——T 50 60 70 hm 80 90 207 100110120130140150160170180190200210 m/z 59.05 41.65% Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 T-r-pn-r-r-[ TrIIIEE nTi 1 59 7.40 7.60 7.80 8.00 m/z 58.05 20.72% 15 31 . 101 83 | mmm ——— T’T TIUTT i s r i f I TEgum mlz->___ 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160170 180 190200210 Abundance #805: Propanal, 2-hydroxy-2-methyl- 43 59 —I—u—TTTuun 7.40 7.60 7.80 8.00 5000 31 m/z 100.95 14.98%

73 88 I1*”! Tpg miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190200210 Abundance #62322: Acetone 43 7.40 7.60 7.80 8.00 m/z 41.00 6.00% 5000 58 27

miz-> mrlmmednp p-rrrp-rrrp rrrpTn ।. !‘1111111111171. (. 1‛Tt 1′1′1117 1‘‘‘I"TT 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 • 4 i ' ’ ‘ • 1 ‘ 1 1 1 I * ‘ ‘ 1 I ' ‘ 7.40 7.60 7.80 8.00

26163.D NP112601.M Mon Dec 03 12:19:11 2001 Page 1

NYC-WTC_000031046

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NYC-WTC_000031046Source: NYC Law Department, mirrored locally

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