GCMS analysis results for sample AD26010, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV2001\26010.D Vial: 3 Acq On : 20 Nov 2001 2:33 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.68 1.40 ug/1 243432 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 2-Pentanone, 4Ahydroxy-4-methyl- 116 C6H1202 000123-42-2 56 2 Acetone / 58 C3H60 000067-64-1 12 3 5-Hexen-2-one 98 C6H10O 000109-49-9 9 4 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 Abundance 7 Scan 287 (7.682 min): 26010.D (-) m/z 43.00 100.00%| 43

5000 59

101 r TTT — TTT ! m/z-> ।■ i m 83 1"111111111" 11 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 ।।।।। . n-i । ri i ■ 111111 207 i" " r m/z 7.40 7.60 59.05 7.80 8.00 48.49% Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- i 43

□ 5000 59 7.40 7.60 7.80 8.00 m/z 100.95 20 ”27% 15 31 101 I I 83 rrprrrprrrrp-r TI) 111" i TIURggu TTTTT |I I I I I U I ! | i1"11 m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200210 'Abundance #62326: Acetone 43

7.40 7.60 7.80 8.00 5000 m/ z 58.05 19.18%- 58 27

m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #1291: 5-Hexen-2-one 1 1 1 1... I ' 1 1 1 I ' f-r 413 7.40 7.60 7.80 8.00 m/z 41.00 7.38% 5000

55 AMWAAd 27 1 69 8398 1 ।11" ।"' ■ i ■ ■" i ■ ■ ■ ■ i ■ TTpT i"•■r■ ■' i" " i miz. 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 7.40 7.60 7.80 8.00

26010.D NP103001.M Tue Dec 11 09:21:47 2001 Page 1

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