GCMS analysis results for sample AD25735, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1601\25735.D Vial: 18 Acq On : 17 Nov 2001 7:37 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 2.28 ug/1 506073 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, ^hydroxy-4-methyl- 116 C6H12O2 000123-42-2 64 2 Acetone / 58 C3H6O 000067-64-1 12 3 5-Hexen-2-G(ne 98 C6H10O 000109-49-9 9 4 Morpholirie, 4-methyl- 101 C5H11NO 000109-02-4 9 \bundance Scan 288 (7.691 min): 25735.D {-) m/z 43.05 100.00% 4p

59 5000

101 ' I I I <

83 7.40 7.60 7.80 8.00 jJj 207 m/z 59. 49.80% m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 21.26% 27 101 I I 83 ,I mfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #62322: Acetone 43

7.40 7.60 7,80 8.00 5000 m/z 58.05 18.66% 58 27 pTTTTrrlbnTTvXmA pTTTpTTTpT-rrpTTTp-TTTJTTTTpTTTp-rTTpTTTyTTTTpTTTpTT^^ m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #63205: 5-Hexen-2-one 43 7.40 7.60 7.80 8.00 m/z 41.05 7721% 5000

55

mZz-> I, , I , , I I I , . , . I I- 1 pYrr I “ . I . . 98 .II...,I.,,,I,.,.I,, ,,I,,,,I,, ,,I,,,,I 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 -p-rn-pTny 7,40 7.60 7.80 8.00

25735.D NP103001.M Thu Nov 29 08:59:13 2001 Page 2

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