GCMS analysis results for sample AD26007, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV1901\26007.D Vial: 17 Acq On : 20 Nov 2001 6:56 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.69 1.29 ug/1 268017 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4 -methyl - 116 C6H1202 000123-42-2 53 2 2-Propanol, -methyl- 74 C4H10O 000075-65-0 12 3 5-Hexen-2-one 98 C6H10O 000109-49-9 9 4 3-Hydroxy-2/pentanone 102 C5H10O2 003142-66-3 9 Abundance Scan 288 (7.686 min): 26007.D (-) m/z 42.9 100.00% 43

59 5000

101 83 7.40 7.60 7.80 8.00 - TTTTTTTTTTTTTT 207 l*"’l i" " r"' i"' ‘ i" " r'111" " I'1" I" " 1111111 m/z !59.05 52.74% m/z--> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 19.79% 15 31 — 101 i 83 | TT‘ |T ..। ।i.... 11. .,.Jip.. ,| I ।111111.. ।.... ।।।।।।. 111. 111111!!! 11' ।!' ।! । u 11 u m/z--> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 210 Abundance #62575: 2-Propanol, 2-methyl- 59

7.40 7.60 7.80 8.00 5000 m/z 58.05 18.04%- 31 41 15

m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 Abundance #1291: 5-Hexen-2-one 43 7.40 7.60 7.80 8.00 m/z 41.05 8.00% 5000 -

55 27 | 69 83 98 . 1." . I..1,... 1 ,i,, ITTTT 111 > 1111 rpri || ■ ■ 1111111! > r 111 r > 11 ■ 1111111 > 11 III 11 > 11111 > ‘TT 1111 > 1111111111! i m/z-> 10 20 30 40 50 60 70 80 90 100110120 130140150160170180190200210 7.40 7.60 7.80 8.00

26007.D GCMS1126.M Wed Dec 12 09:49:22 2001 Page 1

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