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GCMS analysis results for sample AD24697, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24697 with detection of unknown compounds on November 19, 2001.

NYC-WTC_000068825–000068837

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : Cs\HPCHEM\1\DATA\NOV0501\24696.D vial: 17 Acq On : 6 Nov 2001 3:34 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.47 ug/1 242896 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone^z^-hydroxy-4-methyl- 116 C6H1202 000123-42-2 38 2 2-PropanoJ< 2-methyl- 74 C4H10O 000075-65-0 17 3 3-Hydrg;^-2-pentanone 102 C5H10O2 003142-66-3 9 4 Morphpline, 4-methyl-______________ 101 C5H11N0 000109-02-4 9 Abundance Z Scan 288 (7.690 min): 24696.D (-) m/z 43.05 100.00% 4(3

59 5000 101 7.40 7.60 7.80 8.0) 83 1 ‘ ‘ 1 ' ' ' ' 1 ' I ‘ I I I ■ ■ • I ' ra/z 59.05 53.08% nfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275:2-Pentanone, 4-hydroxy-4-tnethyl- 4(3

5000 59 7.40 7.60 7.80 8.00 m/z 101.05 2^747% 15 31 101 1^ , ,1^ I 53 ‘ 1 * ' ‘ ’ 1 ‘ I ' Tlfe-> 10 20 30 40 60 70 80 90 100 110 ^bundance #62572:2-Propanol. 2-methyl- 5^ ..... .. .............................................. 7.40 7.60 7.80 8.00 5000 31 41

1..,....,..^. ,1. ' I ' ‘ ' I ' ' ' ' 1 ' ' ' ' I ' ‘ ‘ ' I ' ' ‘ ' I ' nfe-> 10 20 30 40 50 60 70 80 90 100 110 ^bundanc8 #1691:3-Hydroxy-2-pentanone 3I 59 7.40 7.60 7.80 8.00

5000

15 ..... I ..... I, I...... I t I t . . I 10 I r . 1^. I I ... I 20 30 40 . 45

50 60 , 66 70 73 I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 80 84 90 102 ■ 11 •' ■ I ‘ 100 110 ZZIZ7.40 7.60 7.80 8.00

24696.D NP103001.M Tue Nov 13 12:04:13 2001 Page 3

NYC-WTC_000068835

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NYC-WTC_000068835Source: NYC Law Department, mirrored locally

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