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GCMS analysis results for sample AD24697, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24697 with detection of unknown compounds on November 19, 2001.

NYC-WTC_000068825–000068837

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24696.D vial: 17 Acq On : 6 Nov 2001 3:34 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.54 ug/1 89828 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 intative ID MW MolForm CAS# Qual 1 1,4-DichLe5robenzene-d4 150 C6C12D4 003855-82-1 72 2 Benzen^,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 40 3 Acenaphthylene 152 C12H8 000208-96-8 14 4 4-AipjjQO-2-chlorobenzonitrile_______ 152 C7H5C1N2 020925-27-3 10 Abundance Scan 711 (11.574 min): 24696. D (-) pm/z 149.90 100.00% 1ii0

5000 115 78 52 i'i.^' '11'40' 'iteo' 'I'tM '1'2'00 40 ' ' J I '' ' I ‘ ‘ ' I ' ''I' Tr '' 1 ‘' I' ‘ . . m/z 151.90 . 66.86% TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene<M 1$0

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 37.65% 35 ‘' I' ‘ '' I ' nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592; Benzene-1,2,3.4-d4-. 5.6<lichloro- 1!>0

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 . 23.14%

35 87 I TJTT-n-p I ' I' ‘ ‘' 1' Tife-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #67015: Acenaphthylene 15 2 11.20 11.40 11.60 11.80 12.00 ra/z 52.00 14.75% 5000-

co ... .... I,,..??,, 98 126 I • ' ■ r I I . I I I II . I I h T Tlfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24696.D NP103001.M Tue Nov 13 12:04:15 2001 Page 4

NYC-WTC_000068836

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NYC-WTC_000068836Source: NYC Law Department, mirrored locally

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