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GC/MS analysis results, sample AD24980, November 2001

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Gas chromatography/mass spectrometry analysis of sample AD24980 conducted November 19, 2001, identifying other unknown compounds.

NYC-WTC_000069182–000069192

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0801\24980.D Vial: 9 Acq On : 8 Nov 2001 10:25 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP103001 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.57 0.54 ug/1 118840 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 l,4-Dichlofcobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-]y2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 12 3 Acenaphthylene 152 C12H8 000208-96-8 9 4 Benzaldehyde, 2-hydroxy-5-methoxy- 152 C8H8O3 000672-13-9 9 Abundance / Scan 711 (11.574 min): 24980.D (-) m/z 149.90 100.00% i$o

5000 115 52 78 u. 11.20 11.40 11.60 11.80 12.00 40 Tife-> ' ' I ' '' ' I ' 30 40 nUS 50 60 ,, 70 80 90 ...... . . 110 120 100 130 140 150 160 m/z 151.90 63.46% ^bundance #9593:1,4-Dichlorobenzene-d4 liiO

5000 115 ' I ' ' ' ' I ' ' ' ' I ' ’ 78 1120 11.40 11.60 11,80 12.00 52 m/z 115.00 37.99% 35 ....... II,..?,.......... I,I........... 414^ ■nZj-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Ben2ene-1,2,3,4-d4-, 5,6-dichloro- 1$0

115 11.20 11.40 11.60 11.80 12.00 5000- 52 78 m/z 78.05 20.57%

n/z-> 30 35 I 40 50 Tj-n-rryr 60 70 80 87 I 90 100 A 110 120 130 140 150 160 Abundance #67015: Acenaphthylene J

152 11.20 11.40 11,60 11.80 12.00 m/z 52.00 15.29%

5000

76 ................................ 87 .98 126 ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24980.D NP103001.M Mon Nov 19 12:05:26 2001 Page 2

NYC-WTC_000069191

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NYC-WTC_000069191Source: NYC Law Department, mirrored locally

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