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GCMS analysis results for sample AD24218, Nov 6 2001

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Laboratory report documenting GCMS analysis of sample AD24218 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000068022–000068036

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24217.D Vial: 4 Acq On : 1 Nov 2001 5:57 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.57 ug/1 77694 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 1,4-DicMorobenzene-d4 150 C6C12D4 003855-82-1 47 2 Benze: ^l,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 12 3 Acena ihthylene 152 C12H8 000208-96-8 9 4 iH-py'rrolo[2,3-b]pyridine-2,6-dione 152 C7H8N202! 017384-56-4 9 Abundance Sean 711 (11.575 min): 24217.D (-) Tm/z 149.90 .100.00% 1!i0

5000 115

52 78 11.20 11.40 11.60 11.80 12.00 38 44 I , ,l 87 m/z 151.90 64.25% T Tife-> Abundance 30 40 50 60 70 80 90 100 110 120 130 TSo 150 160 #9593:1,4-Dichlorobenzene-d4 liiO

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 39.91%

TiZz-> 30 35 40 50 UUn I 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592; Benzene-1,2.3,4-44-, 5,6-dichlort>- 1!i0 i'i!aa' '11'40 'iTeo ViSo' 12'00 115 5000 52 78 m/z 78.05 20.62%

Tlfe-> Abundance 35 I 30" "40" ' ' I'''' I' 60 70 4_X_ 80 90 100 110 120 130 140 150 160 #67015: Acenaphthylene 1$2 11,20 11.40 11.60 11.80 12.00 m/z 52.00 . 15.59% 5000

66

' I ' ■ ' ' I ' ' ■ ■ I I • ■ ■ I • TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 1120 1140 1160 1180 12.(X)

24217.D NP103001.M Tue Nov 06 11:46:54 2001 Page 5

NYC-WTC_000068034

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NYC-WTC_000068034Source: NYC Law Department, mirrored locally

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