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GCMS analysis results for sample AD24218, Nov 6 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24218 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000068022–000068036

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24217.D Vial: 4 Acq On : 1 Nov 2001 5:57 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params; LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Butanamide Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 8.66 0.54 ug/1 73009 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 fentative ID MW MolForm CAS# Qual 1 Butanami^^e 87 C4H9N0 000541-35-5 64

s 2 Methy1/15-methoxyhexadecanoate 300 C18H36O3I 000000-00-0 39 3 2-He: .none, 3-hydroxy-3,5-dimethyl- 144 C8H16O2 006321-14-8 39 4 Amyjk :ne Hydrate 88 C5H12O 000075-85-4 39 ^bundanc^ Scan 394 (8.664 min): 24217,D (-)

5000 43

151 .8.^ 8.ro II m/z 42.95 A 37.48%,_> F‘' I ■nZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 ‘\bundance #62880: Butanamide 44 519

□3 5000 8,40 8.60 8.80 9.00 27 72

nfe-> 20 40 UXa 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #42793: Methyl 15-methQxyhexadecanoate 59

8,40 8,60 8,80 9.00 5000 m/z 150.90 8.18%

................ , ,7^ 8/ 111 194 236 253 270 285 I ’ * ‘ ' I ' ' ' ‘ I' ’ ’ ' I I ■ • ■ 111 • r' 1 ‘ ‘ I ' ■nZz-> Abundance 20 40 5b 60 80 100 120 140 160 180 200 220 240 260 280 #8436:2-Hexanone. 3-hydroxy-3,5-dimethyl- A 8,40 8.60 8,80 9.00 m/z 152.90 8.17%

5000 43

I, Ill[, 101 7'........ . y-r-r-n-p-n-rj mfe-> 20 40 60 80 100 120 140 160 180 20) 220 240 260 280

24217.D NP103001.M Tue Nov 06 11:46:52 2001 Page 4 NYC-WTC_000068033

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NYC-WTC_000068033Source: NYC Law Department, mirrored locally

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