GCMS unknown compound analysis, sample AE05515, April 2002

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? Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APRO102\5515.D Vial: 6 Acq On 1 Apr 2002 ■ 4:11 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* ■ Peak Number 5 Butanamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

9.19 42.05 ug/1 7102990 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# . Qual

1 Butanamiide 87 C4H9NO 000541-35-5 72 2 2-Hexan/ne, 3-hydroxy-3,5-dimethyl- 144 C8H16O2 006321-14-8 39 3 3-Hexahol, 3-ethyl- 130 C8H18O 000597-76-2 38 4 Propa/e, 1-ethoxy- 88 C5H12O 000628-32-0 38 Abundance Scan 452 (9.192 min): 5515.D (-) m/ z 59.0 100“. 00 % 3

5000 43

36,1, , 51. 81 8/ 95 107 121 136 151 11 _a8o_aoo__9;2o__9:4o__a^ t m/z 43.0,5 39.74% ■n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #62880: Butanamide 44 5)9

5000 27 8.80 9.00 9.20 9.40 9.60 72 m/ z 41.0 17.24% ' I ' ' ’ ' I ' ' ' ' I I ' I ' ' ' ' I ' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #8436: 2-Hexarione, 3-hvdroxy-3,5-dimethyl-

8.80 9.00 9.20 9.40I 9.60 5000 m/z 150.90 7.91% 43 101 69 83 111 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #65274: 3-Hexanol. 3-ethyl- / 9 8.80 9.00 9.20 9.40 9.60 m/z 152.90 7,51% 5000

31 70 83 101 11 « I I I n-'' '-'T^ nn/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 8.80 9.00 9.20 9.40 9.60

5515.D GCMS0403.M Thu Apr 04 13:53:08 2002 Page 5

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