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GCMS analysis results for sample AE04131, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AE04131 conducted on April 1, 2002.

NYC-WTC_000011817–000011832

Folder label: “GCMS X 2/25/02 A 3/23/02”

←Page 12 of 16→
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2202\4131.D Vial: 27 Acq On : 23 Mar 2002 9:42 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Butanamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

9.21 76.55 ug/1 8788030 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butanamide 87 C4H9NO 000541-35-5 64 2 3 - Hydroxy - 3 - me t hyl - 2 - but anone 102 C5H10O2 000115-22-0 50 3 2-Hexanone, 3-hydroxy-3,5-dimethyl- 144 C8H1602 006321-14-8 39 4 2-Propanol, 2-methyl- __ 74 C4H10O __ _ 000075-65-0 36 Abundance Scan 454 (9,215 min): 4131 .D(-) m/z 59.05 100.00% 59

5000 43 ****1’4*14’1** 8.80 9.00 9.20 9.40 9.60

m/z-> ---35 10 20 30 40 51 TTTr 50 60 . ■ . 9 ■ . 80 87, 95, ! . 107 .... 123 . । 130, . . . 177 . 70 80 90 100 110 120 130 140 150 160 m/z 43.05 41.64% Abundance #62880: Butanamide 44 59

5000 8.80 9.00 9.20 9.40 9.60 27 72 m/z 41.0,5 17.58% I. 67 1111—010002u0uunmmunuuumOannnor ■ ■ i ■ ■ ■ • i ■ • ■ ■ i ■ ■ • • i"'1'* • i ■ ■ ■ • i ■

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance .? 3- d-w ytl , e 59

8.80 9.00 9.20 9.40 9.60 5000 31 m/z 150.90 8.08% ; 43 15 69 87 102 T—0Emuu—*pmotmtOGpTtdt -p-T-n-p-TT-ry r11' 'i ""i TTT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #8436:2-Hexanone, 3-hydroxy-3,5-dimethyl- 59 8.80 9.00 9.20 9.40 9.60 m/z 152.90 7.60% 5000 43 101 83 I 111 69 m/z~> usidpus ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i1 ■ ■ ‘ i1 ■ ■ • i ■ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ' ■ i ■ ■ “ i " ■' i ■' •111 ■ “ i ■ ■ ‘ 1“ i ■ • ■' i ‘1 ■' i1 ■ 8.80 9.00 9.20 9.40 9.60

4131.D GCMS0308.M Wed Mar 27 10:10:04 2002 Page 5

NYC-WTC_000011828

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NYC-WTC_000011828Source: NYC Law Department, mirrored locally

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