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GCMS analysis results for sample AD24236, Nov 5 2001

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Laboratory report documenting GCMS analysis of sample AD24236 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068070–000068084

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24220.D Vial: 7 Acq On : 1 Nov 2001 8:52 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Butanamide Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 8.67 0.59 ug/1 92471 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butanal de 87 C4H9NO 000541-35-5 64 2 2-Hexi one, 3-hydroxy-3,5-dimethyl- 144 C8H16O2 006321-14-8 39 3 3-He: 5nol, 3-ethyl- 130 C8H18O 000597-76-2 39 4 1-B' anol, 3 -methoxy-104 C5H12O2 002517-43-3 39 Abundance Scan 395 (8.673 min): 24220.D (-) m/z 5^705 100.00% Sb

5000 43

153 8.40 8.60 8,^ 9^,, 109 JJL Wt ‘ ’ p • I»j I I 11 I I I''' 'I' p- T m/z 42.95/ 35.75% ) n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #62880: Butanamide 44 53

5000 8.40 8.60 8.80 9.00 27 m/z 41.05 16721% 72

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #8436:2-Hexanone, 3-hydroxy-3,5-<limethyl- 5b 8.40 8.60 8.80 9.00 5000 m/z 152.80 8.12% 43 ft 101

Tife-> JJ ' I'''' r ‘ ‘ ‘ 69 83 ''' I' I 111 " " I''n 2) 30 40 50 «) 70 80 90 100 110 120 130 140 150 160 ' I ' ' ' ' I ' ' ' ‘ I P^^H

Abundance #65274:3-Hexanol. 3-ethyi- 8.40 8.60 8.80 9.00 m/z 69.00 7.44% 5000

Tife-> 20 II 31

30 40 45 50 60 70 83 101 -I...80. 90 100 110 120 130 140 150 160r 70 I ‘ I ' ‘ ‘ ‘ I' ‘' I ‘ ‘ ' I ‘‘ ‘ I ' ' ‘ ‘ I ■ ■' 8.40 ' I'- 8.60 8.80 9.00 i 24220.D NP103001.M Tue Nov 06 11:51:17 2001 Page 4

NYC-WTC_000068081

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NYC-WTC_000068081Source: NYC Law Department, mirrored locally

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