GCMS analysis results for sample AE04129, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2202\4129.D vial: 25 Acq On : 23 Mar 2002 7:44 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Butanamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

9.20 19.60 ug/1 2265560 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butanamide / 87 C4H9NO 000541-35-5 72 2 3-Hydroxy- i -methyl-2-butanone 102 C5H10O2 000115-22-0 50 3 2-Hexanone 3-hydroxy-3,5-dimethyl- 144 C8H1602 006321-14-8 40 4 3-Hexanol, 3-ethyl- 130 C8H180 000597-76-2 39 Abundance ....... t ..............Scan 452 (9.198 min): 4129.D (-) m/z 59 05 100.00% 59

5000 43

51., , 69 80 87 95 107 123 138 151 8.80 9.00 9.20 9.40 9.60 ................... fnfiWi m/ z 43.0,5 40.42% m/z-> 10 20 30 40 50 ।60 70 80 90 100 110 120 130 140 150 160 Abundance #62880: Butanamide 44 59

5000 ■ i • ' 1 ' I ■ • i • ■ ■ ■ i ■ r

27 8.80 9.00 9.20 9.40 9.60 72 m/ z 41.0,5 17.72% TT ‘ I “"i, 87 ‘i ‘i■ ■ ■■ i ■ ■ ■■ i" i■ ■ ■■ i ■ ■ “i■■ ■■ TTI111' m/z-> ' 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance *847 7 3-Hvdroxy-3-mtettyl2-butanene 59 ............. ...... 1 8.80 9.00 9.20 9.40 9.60 5000 31 m/z 150.9,0 8.17% 43 15 69 87 102 T’I’TT’I’-2T:-’1111’1"1"’TT’’TT1’101111’11111112111003TE 1111111 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #8436:2-Hexanone, 3-hydroxy-3,5-dimethyl- 59 8.80 9.00 9.20 9.40 9.60 m/z 152.90 7.61% 5000 43 101

miz-> 1 IT69 | 111 ■ i ‘■ i ■ ■ ■ ■ i ■ ■" i1 •»■ i ■ 83 ।।।।111111111111 11,11111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 8.80 9.00 9.20 ' 9.40 " 9.60 '

4129.D GCMS0308.M Wed Mar 27 10:06:36 2002 Page 6

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