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GCMS analysis results for sample AE04129, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AE04129 conducted on April 1, 2002.

NYC-WTC_000011800–000011816

Folder label: “GCMS X 2/25/02 A 3/23/02

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Scanned page image, NYC-WTC_000011811
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2202\4129.D Vial: 25 Acq On : 23 Mar 2002 7:44 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Butane, 2,2,3,3-tetranitro- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

8.30 0.54 ug/1 62238 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2,2,3, 3-tetranitro- 238 C4H6N4O8 020919-97-5 25 2 2-Propanone, ,1,1-trichloro­ 160 C3H3C130 000918-00-3 25 3 2-Propanone, ' 1,1-dichloro- 126 C3H4C120 000513-88-2 17 4 N-Acetylpyrr olidone 127 C6H9NO2 000932-17-2 5 Abundance " ‘ Scan 354 (8.299 min): 4129.D(-) i m/z 43.00 100.00% 43

5000

37 49 63 7-1 83 97 i । .. 125 117, I i 8.00 8.20 8.40 8.60 TIIPP ' i-| । ■ » i f.'i । . | . ... । Ih'i 1 m/z 124.8,5 10.64% m/z-> 10 20 30 40 50 60 70 80 S90 100 110 120 130 Abundance #31332: Butane, 2,2,3,3-tetranitro- 30 43

5000 * ’ ’ I ’ ’ ’ • I ‘ M 1 1 1 | 1 1 ’ ‘ 8.00 8.20 8.40 8.60 53 m/z 46.9,5 6.87% 15 - miz-?____ 10 20 —37+ ------------------ 30 40 50 60 70 80 90 100 110 120 130 Abundance 212/47 -fppapine 43 MAAAAAMAAAAAAAs 8.00 8.20 8.40 8.60 5000 m/z 82.95 6.86%

15 35 49 85 97 117 125 ■1 i ■ ■••1111 1111 1 11 11 1 > । 11 1111 1 I ' 1 11 I'11 ■ i ■ ■ ■ <‘l ■ ■ ■ * i ■ • । i i 11»i m/z-> 10 20 30 40 50 60 70 90 10080 110 120 130 Abundance #64841:2-Propanone, 1,1-dichloro- 43 8.00 8.20 8.40 8.60 m/z 126.9,0 6.60% 5000

27 I . 35 49 63 83 91 126 • ’ I • ’ ‘ ■ l 1 1 1 1 1 1 1 ‘ 1 1 1 1 ‘ 1 i ■ 1 ' ' i ■'■ ■ ■ i ' 1 • ■ i ‘ 11’11+11+***1**’1III ' I ■ • ■ • i ■ ■ • ■ i ■ ■ ■ ■ i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 8.00 8.20 8.40 8.60

4129.D GCMS0308.M Wed Mar 27 10:06:32 2002 Page 5

NYC-WTC_000011811

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NYC-WTC_000011811Source: NYC Law Department, mirrored locally

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