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GCMS chromatogram data for sample AE04590, April 2002

Machine-extracted title · confidence 100%

Analytical run record from April 2, 2002, documenting unknown compounds and surrogate recovery for sample AE04590.

NYC-WTC_000058372–000058381

Folder label: “GCMS X 3/4/02 A 3/26/02

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Scanned page image, NYC-WTC_000058380
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR2602\4590.D Vial: 6 Acq On 26 Mar 2002 2:39 pm Operator: Sample gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) ■Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.28 0.35 ug/1 54670 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 - Propanoine, 1,1,1 - trichloro- 160 C3H3C13O 000918-00-3 45 2 2-Propanone, 1,1-dichloro- 126 C3H4C12O 000513-88-2 9 3 1-Fluorononane 146 C9H19F 000463-18-3 9 4 1-Octadecariol 270C18H38O 000112-92-5 9 Abundance ’ Scan 353 (8?283 min): 45907d (’-) m/ z 43/00..... 100700% 4|3

5000

.49 63 5,3 97 119125 8.00 8.20 8.40 8.60 ' I ' ' ' '1 ‘ ‘ ' I ‘ « I ' 1 m/z 124.85 8.41% 'm/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 8.00 8.20 8.40 8.60 15 m/z 96.85 ' 7.02% , I, 35 49 85 97 U7 125 ' ' I ' '' m/z-> 10 20 30 40 50 61 70___ 80__ 90 100 110 120 130 Abundance #64841: 2-Propanbne. f’-aicnlc-u- 43

8.00 8.20 8.40 8.60 I 5000 m/z 42.05 6.84% I ! 27 i 36 49 63 83 91 .......... 126

Abundance I ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 10 20 30 40

43 50 60 70 #8922: 1-Fluorononane 80 90 100 110 120 130 1^,., I 8.00 8.20 8.40 8.60 m/z 82.85 6.61% 5000 56 27 70 84 97

'm/Z“> 10 20 30 33 40 I 50 I 60 70 I 80 90 100 110 120 130 A 8.00 8.20 8.40 8.60

4590.D GCMS0308.M Thu Mar 28 16:25:25 2002 Page 2

NYC-WTC_000058380

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NYC-WTC_000058380Source: NYC Law Department, mirrored locally

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