GCMS analysis results for sample AE06634, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR16O2\6634.D Vial: 7 Acq On : 16 Apr 2002 7:04 pm Operator: Sample : gc/ms scan 3/22 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************* * * ********************** Peak Number 1 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 8.25 0.30 ug/1 40211 1,4-Dichlorobenzene-d4 12.22

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanoney 1,1,1-trichloro- 160 C3H3C13OI 000918-00-3 78 2 2-Propanone/ 1,1-dichloro- 126 C3H4C12OI 000513-88-2 9

./ft. 3 Butanoic acid, 2-acetyl-3-methyl-, 158 C8H14O3 051756-10-6 9 4 4-Penten-^one 84 C5H8O _____ 013891-87-7 7 Abundance ' Scan 349 (8.251 min): 6634.D (-) 4)3

553

8.00 8.20 8.40 8.60 37 , ,49 . ■‘r^e-T^-r-r-r-iy-e-r-r-r-^^r-r-rT-jVVT-^-y-r-r-e-ey-r-r-r-TYr-r^^ m/z 124.85 8.00% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone. 1,1,1-trichloro- 4)3

5000 nu, 8.00 8.20 8.40 8.60 m/z 82.95 6.70% 15 I ' I ' ' ' ' I ' 35 ■ ''' ' 1.' 49 85 97 ''i ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ‘ ''' I ' ‘ 117 125 ' I ' ' ' ' I ' ' ''' I ' Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4368: 2-Propanone, 1,1-dichloro- 4)3 A 8.00 8.20 8.40 8.60 5000 m/z 126.90 6.16% A 15

m/z-> 10 I 20 7^ ' ' I ‘ 30 40 ' I ' 49 63 50 60 70 80 90 100 110 7g 83 93 120 130 Abundance #11890: Butanoic acid, 2-acetyl-3-methyl-, methyl ester 4)3 8.00 8.20 8.40 8.60 m/z 83785 5721% 101 5000 116 15 69 i 27 59 84 127 I I 33 ■nfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 8 00 8 20 fl 40 fl RO

6634.D GCMS0412.M Wed Apr 17 12:02:27 2002 Page 1

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