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GCMS analysis results for sample AE06634, April 2002

Machine-extracted title · confidence 100%

DEP laboratory report of GCMS analysis for sample AE06634 conducted on April 18, 2002.

NYC-WTC_000060468–000060477

Folder label: “GCMS X 3/21/02 A 4/16/02

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Scanned page image, NYC-WTC_000060476
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1602\6634.D Vial: 7 Acq On : 16 Apr 2002 7:04 pm Operator: Sample : gc/ms scan 3/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator)’ Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 14.82 7.27 ug/1 1244350 Naphthalene-d8 15.84 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 CyclopentasiLoxane, decamethyl- 370 C10H3005Si5 000541-02-6 2 3,4-Dihydroxymandelic acid, ethyl e 428 C19H36O5Si3 000000-00-0 47 3 Benzenemeth^ol, .alpha.-(aminometh 369 C17H35NO2Si3 056145-08-5 38 4 Benzoic acW, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 38 Abundance / Scan 1064 (14.815 min): 6634.D (-) m/ z 73.00 100.00% 73

267 355 5000 M 45 108 133 154 175193 223 249 293 323 |[ 14.40 14.60 14.80 15.00 15.20 0 ' ‘' I''" I'' I" " i'' MI" I'"' I "1'' I " I" " I" " I ‘' n " " I" " I" " I' m/z 355.05 57.21% Ti/z-> 40 60 80 100 120140 160180 200 220 240 260 280 300 320 340 360 380 400 Abundance , #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 267.00 51.89% 207 249 323 , Il I' ' I' ‘ ‘ I I"'' I' "' I' " ' ' I' " ' I ‘ H " i n/z-> 40 60 80 100 120 140 160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #55759: 3,4-Dihydroxymandelic acid, ethyl ester, tri-TMS 3$5

73 H \ 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.05 19760% A 208 251 281 385 413 pTTTTTTTTyrTTTpTTTyrrTTp-rrrp-rV^^ ' 1" " I " ' I' ■nfe-> Abundance 40 60 80 100 120140 160180 200 220 240 260 280 300 320 340 360 380 400 #51228: Benzenemethanol, .alpha.-(aminomethyl)-4-hydroxy-, 2$7 n 14.40 14.60 14.80 15.00 15.20 73 102 m/z 357.05 13.07% 5000

193 237 354 pTT-TTTTTTTTTTVp-TTTpTTT^^ i -n/z-> 40 60 80 100 120140 160180 200 220 240 260 280 300 320 340 360 380 400 14.40 14 60 14 80 15 00 15 20

6634.D GCMS0412.M Wed Apr 17 12:02:28 2002 Page 2

NYC-WTC_000060476

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NYC-WTC_000060476Source: NYC Law Department, mirrored locally

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