GCMS analysis results for sample AE08015, April 2002

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Laboratory report documenting GCMS analysis of sample AE08015 conducted on April 24, 2002, including surrogate recovery data.

NYC-WTC_000047691–000047700

Folder label: “GCMS X 4/4/02 A 4/12/02”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\1\DATA\APR1102\8015.D Vial: 21 Acq On : 12 Apr 2002 10:03 am Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 14.83 0.24 ug/1 38477 Naphthalene-d8 15.86 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 3,4-Dihydrokybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 40 3 Benzoic ac 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 33 4 Phenethylamine, N-methyl- .beta. , 3,4 3 99 C18H3 7NO3Si3 010538-85-9 32 Abundance Scan 1065 (14.826 min): 8015.D (-) m/ z 73.00 100.00% 73

5000 267 355 .................. \.................. 1 1 ' ' 1 ] 1711 । | । T r । [ i 1 i i | i > 14.40 14.60 14.80 15.00 15.20 .... 45 1...... 125 154 ...........2^1,,.... — m/z 267.00 40.52% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.05 37.30% 323339 ’ U" 11n1,0’0—unt——p—uu—191207 n’’TT Tpu 251 | T’T 1Tn m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73

14.40 14.60 14.80 15.00 15.20 5000 267 m/z 356.05 14.14% 179 356 45 147 | 237 , , 209 312 341 1 111 ‘11 ' 11"111'' 1 11" " i11 r 1 i" f-p-r " ' i "r ■ i ■ " i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #72300: Benzoic acid, 2-[(trimethylsilyl)oxy]-, trimethyisi | 1 1 1 1 | ' ' ■ 1 | 1 ' > ' | ■

73 14.40 14.60 14.80 15.00 15.20 m/z 267.90 11.42% 267 5000

45 1 92 135151 175 193209 233249 , 11 I ’T । | । । । i ] । । I1 । | i i*-i i | । ri । | I i I I | ITI I | i i i I I I I I I I I I I y 1 1 1 I I I I

m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

8015.D GCMS0412.M Tue Apr 16 12:07:36 2002 Page 1

NYC-WTC_000047698

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