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GCMS analysis results for sample AE07318, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE07318 conducted on April 10, 2002.

NYC-WTC_000046673–000046682

Folder label: “GCMS X 3/28/02 A 2/27/02

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Scanned page image, NYC-WTC_000046681
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR0302\7318.D Vial: 14 Acq On 4 Apr 2002 1:33 am Operator: Sample gc/ms scan 3/28 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 14.84 1.67 ug/1 252847 Naphthalene-d8 15.88 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 (90 2 Phenethylamine, N-methyl-.beta. , 3,4 399 C18H37NO3Si3 010538-85-9 38 3 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 37 4 N- (Trifluoroacetyl) 2 -N,O,O' ,0' 1-tetr 553 C22H42F3NO4Si4 000000-00-0 32 Scan 1067 (14.844 min): 7318.D (-) Abundance m/ z 73.00 100.00% 73

5000 267 355

45 108 133 154 177 193208223 251 | 14.60 14.80 15.00 15.20 323339 L 1 1TI ■' 1 I ■ ■ ■ ■ i TTmPTmTPTmP, ITMIIanii n m/z 267.00 44.56% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 5000 267 1I ► | » 1 1 1 | , T

14.60 14.80 15.00 15.20 m/z 355.05 44.46% 191207 323339 m/z-> ’' i1' ■111 nnauns 1‘T i' " 111'1' i 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73 —----- 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 15.98% ft 44 I 188 130147 193 267 294 1' i " TT+ 11—000 mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 - Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 14.60 14.80 -15.00 15.20 m/z 2 68.00 11.42 267 5000 179 356 45 147 209 237 . | 312 341 / i । ■ ■ ■ ■ । ■ ‘‘‘‘‘I ——00— i ' ' ' ' i ' ' 1 ■ i' 1 1 T’r i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.60 14.80 15.00 15.20

7318.D GCMS0403.M Tue Apr 09 13:09:06 2002 Page 2

NYC-WTC_000046681

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NYC-WTC_000046681Source: NYC Law Department, mirrored locally

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