Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
NYC-WTC_000039588–000039610Folder label: “GCMS X 3/19/02 A 4/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C : \HPCHEM\ 1 \DATA\APR1 702\6455.D Vial: 13 Acq On : 17 Apr 2002 7:57 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 4 Cyclopentasiloxane, decamethyl Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T. 14.81 1.34 ug/1 195478 Naphthalene-d8 15.85
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane/ decamethyl- 370 C10H3005Si5 000541-02-6 49 2 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 3 N- (Trifluoracety]) -0,0' ,O”-tris (tri 495 C20H36F3NO4Si3 000000-00-0 38 4 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 38 Abundance Scan 1064 (14.811 min): 6455.D (-) m/z 73.00 100.00% 73
5000 267 355
45 14.40 14.60 14.80 15.00 15.20 108 133154 193 223 „ ( - .............. 323 I T*1n l' l -i Tnd.T । । TI m/z 355.05 49.84% m/z—> 50 100 150 200 250 300 350 400 450 500 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 .... - 5000 14.40 14.60 14.80 15.00 15.20 m/z 267.00 48.46%
m/z—> ■ 1 i 50 ............................. 207 100 150 200 —2 250 300 350 400 450 500 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73
14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 17.43% J mz— > LL_ 44 147 193 267 294 350 | T TI . 17 "II ■ 1 ■ 'i > ■ ■ ■ i ■ ■ ■ ■ i ■ '■ ■ ■' । ■ ■ ■ ■ । । 1 ■ ■ । 50 100 150 200 250 300 400 ■
450 I । । 1 1
500 1 ।
- Abundance #58807: N-(Trifluoracetyl)-O,O‘,O"-tris(trimethylsilyl)epin 73 14.40 14.60 14.80 15W 15.20 355 m/z 268.00 13.85% 5000
45 1 140 184 —_ 1__1_ t—__1__ 1_ 1 — 281 ----- I, । , ! I I I 480 II TI ' [ । । । । | i । i TI 1 i । I । । i ! I । r T miz-s 50 100 150 200 250 300 350 400 450 500 14.40 14.60 14.80 15.00 1 5.20
6455.D GCMS0412.M Thu Apr 18 09:14:15 2002 Page 4
NYC-WTC_000039598
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039560
Laboratory report documenting GCMS analysis of sample AE06453 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039574
Laboratory report documenting GCMS analysis of sample AE06454 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047979
GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000060478
DEP laboratory report of GCMS analysis for sample AE06635 conducted on April 18, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000039437
Department of Environmental Protection site log sheet for the World Trade Center area covering March and April 2002.
Filed in the same folder
NYC-WTC_000039438
Fragmented page from a GCMS record series dated April 2002 within DEP Box 23 archives.
Filed in the same folder
NYC-WTC_000039441
Calibration report for GCMS analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039445
Laboratory report documenting GCMS reference analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder