GCMS calibration results for sample AE09585, May 2002

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0 3 02\9585.D Vial: 12 Acq On 4 May 2002 12:49 am Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.79 3.48 ug/1 280963 Naphthalene-d8 15.83 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 2 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 33 3 N-(Trifluoracetyl)-0,O1,O"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 28 4 Benzeneeth amine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 28 Abundance Scan 1064 (14.791 min): 9585.D (-) m/z 73.10 100.00% 73 A 5000 267 355 1 ' i ' 1 1' । ' 45 14 40 14.60 14.80 15.00 15.20 III 103125 154 193 223 , , 323 _ i ‘‘I’’ —I| 11 । 113 । r । I i ’ । " । J" 11 । i | I i i I । 1 । i r | 1 m/z 267.05 29.16% m/z->_______ 50 100 150 200 250 300 350 400 450 500 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 I । i i i i । i । i 4 । i i i । । । i i i । i r 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.10 25.56% ... ............207 . 323, m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy}-, trimet 73 355 ----- ' ' i ' 1 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.10 9.21%

147 267 47 ... 208 ^7 1 ■ ■ i ■ ■ ■ ■ । ■ ■ l ' 1 m/z—>_____ 50___ 100 150 200 250 300 350 400 450 500 Abundance #58807: N-(Trifluoracetyl)-O,O',O"-tris(trimethylsilyl)epin ___________ __________ 1 i ■ 1 1 1 i 1 ' 1 1 1 1 ' 1 ' i 1 1 1 1 1 1 1 73 14.40 14.60 14.80 15.00 15.20 355 rn/z 74.10 8.79%|

5000-

45 | 140 184 281 480 Tl /............. ■ 1 ■■ i ■ 1 1 1 ' 1 r [ 11“ i । i | I I I I [ T m/z-> 50 100 150 200 250 300 350 400 450 500 14.40 14.60 14.80 15.00 15.20

9585 .D GCMS0501.M Mon May 06 10:50:44 2002 Page 3

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