GCMS calibration table for method GCMS0412, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR1102\8016.D Vial: 22 Acq On : 12 Apr 2002 11:02 am Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 14.83 0.77 ug/1 120271 Naphthalene-d8 15.86 Hit# of 5 Tentative ID MW Mol Form/j CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H30O 5Si5 000541-02-6 2 N- (Trifluoroacetyl) -N,O,O' ,0' ‘-tetr 553 C22H42F3NO4S14 000000-00-0 47 3 Benzoic acid, 2,4-bis [ (trimethylsil 370 C16H3004Si3 010586-16-0 47 4 N-(Trifluoijacetyl)-O, 0 1 ,0"-tris (tri 495 C20H36F NO4 13 000000-00-0 38 Abundance Scan 1066 (14.832 min): 8016.D (-) 73.00 100.00% 73

267 355 5000

45 14.60 14.80 15.00 15.20 I । 125 154 191 223 1 [ 323 r 1 i 1 1 i i — | i i i r ‘i । " " | ' i r' i *l -- 1 1 1 P— । । T । ~t_ ।_ ।—। । । । । । । । । । । । m/z 355.05 50.01% n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 ‘ I’’ 14.60 14.80 15.00 15.20 m/z 267.00 49.76% 207 323 — ———————— m/z—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethylsi 73

355 14.60 14.80 15.00 15.20 5000 m/z 356.05 17.18%

45 I, ' 1 i 1 ' 147 193 267 538 — 1[B——ddm——n—UVETBDCT-—B-B-T/1 n/z->_____ 50 100 150 200 250 300 350 400 450 500 550 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet i 1 ' ' 1 i 73 14.60 14.80 15.00 15.20 m/z 267.90 12.76% 5000 355 45

133, 1 93 223 281 ________ A_____________ ‘‘I ‘ i i— i y II i r [ i i “ i— i | i i

m/z—> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

8016 .D GCMS0412.M Tue Apr 16 12:08:06 2002 Page 3

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