GCMS analysis results for sample AE06993, April 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\APR0405\6993.D Vial: 22 Acq On 6 Apr 2002 4:36 pm Operator: Sample gc/ms scan 3/26 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 14.85 1.40 ug/1 110450 Naphthalene-d8 15.88 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 74 2 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 58 3 p-Trimethylbilyloxyphenyl-bis(trime 370 C17H3403Si3 000000-00-0 38 4 N- (Trifluoracetyl) 0,0’,0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 37 Abundance Scan 1068 (14.847 min): 6993.D (-) m/z 72.95 100.00% 73 fl

267 355 5000

' ‘ l ' ' 14,60 14.80 15.00 15.20 45 103 ’1111 I I j l 1 II 11II IAT 133 154170 193 1 1' '' ] 223 21.... 11'' 'I — I — 3 1 I I 1 II I I 323339 I 1iiI I [I I T 1111 1 i । 1 t 1 1 '| 1 1 1 I’’ m/z 355.05 53.55% mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 ' 1 I 1 1 ' 1 I ' 1 14.60 14.80 15.00 15.20 m/ z 2 67.00 53.37% 191207 251 |, 323339 ’ 1’ i111' ।111' j ■1111 " 11111 >11 • ’ ■ 'i ■ TTr ■ i ■ ■ ■ i > ■ ■ ■

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyl alcohol, tris(trimethylsilyl)- 73

14.60 14.80 15.00 15.20 5000 267 m/ z 35 6.05 19.45% 179 356

m/z-> 40 L 45

1’1111117 60 111111 147 1 ....... ...... 209 237 |,........ 312 341 L "II’ITTT 1 | 1 1 1 I j 1 1 1 1 | 1 I I I ( I J I I' | I I T I | I N I ] I I I 11’01111111111 ITT 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51305: p-frimethylsilyloxyphenyl-bis(trimethylsilyloxy)eth 1 1 I 1 1 1 1 1 1 ' ■ i ■ ■ ' ■ i ' ■ 267 14.60 14.80 15.00 15.20 73 m/ z 2 68.00 14.82%

5000

147 45 119 _......... .......... TTTTT 177193 251 355 1 • i1 ’'1 r ■11 r n 11 1111 "111111 " 1111111 lJ 11111 111000—0—0—1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.60 14.80 15'00 15.20

6993.D GCMS0408.M Mon Apr 15 14:44:03 2002 Page 1

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