NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\APR0405\6992.D Vial: 21
Acq On 6 Apr 2002 2:37 pm Operator:
Sample gc/ms scan 3/26 Inst : GC/MS 209
Mise Multiplr: 2.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
14.85 1.95 ug/1 157843 Naphthalene-d8 15.88
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H30O5S15 000541-02-6 76
2 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 58
3 3,4-Dihydroxymandelic acid, ethyl e 428 C19H3605Si3 000000-00-0 47
4 Phenethylamine, N-methyl-. beta. , 3,4 399 C18H37NO3Si3 010538-85-9 43
Abundance Scan 1068 (14.847 min): 6992.D (-) m/z 73.00 100.00%
73 ft
267 355
5000
1 ‘ i 1 1 1,tI 1 1 1 ‘ | 1 1
45 14.60 14.80 15.00 15.20
125 154 191 223 249 1 323
TTT i''" i TTT T Tr T to 1 । t'i 11 j 111 i' 11 rf i । t TT TTTTTT TT L 11''1111 ■ ‘ 11 m/z 355.05 50.24%
mlz-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267 ....... /
5000 1 ' 1 1 1 1 1 r 1 ‘ ' ' i ‘ 1 ' ' i ’ 1
14.60 14.80 15.00 15.20
m/z 267.00 48.75%
|
, ________ ___________ 207 249 |,__ 323
I‘ ' 1 1 ' ‘ ' I " " I " " I TTI l-l u | ) I -I J ] m J | ! J 1 l | l j”l ! | ! T TTT TTTTTTTT
111111'1111111111
mz-> 40 60 80 100 120 140160 180 200 220 240 260 280 300 320 340 360 380 400
Abundance #49868: 3,4-Dihydroxybenzyl alcohol, tris(trimethylsily!)-
73
1 1 1 * ‘ 1 ' 1 * 1 T-T-p-T-r-r-|-r-r
14.60 14.80 15.00 15.20
267 m/z 356.05 18.03%
5000
179
356
147
209 237 , , 312 1
mlz—>
T
‘1‘111111111111111—01"T11101T1"
I " i " " i" ' HT 11'1 '11
40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400
Abundance #55759:3,4-Dihydroxymandelic acid, ethyl ester, tri-TMS
1 ’ 1 1 1 1 ’ 1 1 1 ’ I 1 1
355 14.60 14.80 15.00 15.20
m/z 268.00 11.81%
73
5000
208 251 281 , 385 413
‘I‘ ‘"7‘11711/1/111111—1"17771m7111111111111111111111111111111111111111111111111117 1111’111,111,1,111
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 14.60 14.80 15.00 15,20
6992.D GCMS0408.M Mon Apr 15 14:43:52 2002 Page 1
NYC-WTC_000040144
OCR can misread numbers and units. Confirm readings against the page image before using them.