NYC-WTC_000039560
Laboratory report documenting GCMS analysis of sample AE06453 conducted on April 19, 2002, by the DEP.
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 13 pages
GCMS surrogate recovery data for sample AE06423, April 2002
Machine-extracted title · confidence 100%Surrogate recovery data for sample AE06423 analyzed by GCMS on April 18, 2002.
NYC-WTC_000039681–000039693Folder label: “GCMS X 3/19/02 A 4/5/02”
Page image
OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
4 Library Search Compound Report
Data File C:\HPCHEM\1\DATA\APR0405\6423.D Vial: 9 Acq On 5 Apr 2002 7 : 54 pm Operator: Sample gc/ms scan 3/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 14.85 0.54 ug/1 82017 Naphthalene-d8 15.88
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H30O5S15 000541-02-6 2 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 52 3 Phenethylamine, N-methyl-.beta. , 3,4 399 C18H37NO3Si3 010538-85-9 43 4 3,4-Dihydrojxymandelic acid, ethyl e 428 C19H3605Si3 000000-00-0 38 Abundance Scan 1068 (14.847 min): 6423.D (-) m/z 73.00 100.00% 73
267 355 5000-
■ ■ i • ■ ■ • i > ■ 45103 133 154 1 93 223 249 । 14.60 14.80 15.00 15.20 323 , I m/ z 2 67.00 52.42% HH TTETu T n " ‘1 " i t TI rr ।' । ■' । TI T Tt 11111 " r 1 mte-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 5000 267 / \ [ 1 ' 1 1 i TIT 14.60 14.80 15.00 15.20 m/z 355.05 52.00%
i"" i1 ■111 207 i• "i 2491 i1 n 1111111 323.4 111 " 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #49868: 3,4-Dihydroxybenzy! alcohol,tris(trimethylsilyl)- 73 ■ ■ I 1 ■ ■ ■ i ' ■ ' ' i 1 ' ' 1 i 1 ' 14.60 14.80 15.00 15.20 267 m/z 356.05 19.37% 5000 179 356 45 147
‘ T I , r'11 r 111 r 11 ■ i ■" 11 I,T’I’ 209 237 , TITO ‘II 312 i' “ ' r 1" f1' ITL " •' i ’' " i " m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #74238: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 11 l 1 355 14.60 14.80 15.00 15.20 73 m/z 267.90 14.07%| | 5000-
130147 179i i T I | [ > I i i | l i i i | r i'i i j i Vf i | i i i i 265 294 i i i i j i i i i । i i ‘i i | i"i i i |' i I I i | 384 i11" i1 I" "I ""I" 1 1 i ' 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 14.60 14.80 15.00 15.20
6423.D GCMS0408.M Wed Apr 10 12:23:12 2002 Page 1
NYC-WTC_000039688
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