NYC-WTC_000039560
Laboratory report documenting GCMS analysis of sample AE06453 conducted on April 19, 2002, by the DEP.
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 13 pages
GCMS surrogate recovery data for sample AE06423, April 2002
Machine-extracted title · confidence 100%Surrogate recovery data for sample AE06423 analyzed by GCMS on April 18, 2002.
NYC-WTC_000039681–000039693Folder label: “GCMS X 3/19/02 A 4/5/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\l\DATA\APR0405\6423.D Vial: 9 Acq On 5 Apr 2002 7:54 pm Operator: Sample gc/ms scan 3/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 38.82 0.66 ug/1 37278 Perylene-dl2 37.93
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3,6-Dioxa-2,4,5, 7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 25 2 Benzophenone ,41,5-tricarboxylic a 356 C19H1607 000000-00-0 10 3 2,6-Dimethyl'- 3,4-bis (trimethylsilyl 311 C15H29NO2Si2 000000-00-0 10 4 1,3-Benzodioxole, 5- [3-acetaminopro 221 C12H15NO3 000000-00-0 9 Abundance Scan 3679 (38.817 min): 6423.D (-) m/z 73.00 100.00% 73 /
147 221 5000 281 355 96 429 40 I 38.40 38.60 38.80 39.00 39.20 m"I || 253 | ... TH ‘ ' I" " I" 'p'"11 .. 41... ...... I 11" " i" " I m/z 147.00 61.35% miz-> ___40 60 80 100120140160180200220240260280300320340360380400420 Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 221
73 5000 AA , AMA, AAL , MyA AAA 38.40 38.60 38.80 39.00 39.20 191 m/z 221. 5 53.65% 117 279
mlz-> ... LL I • " 111 • 11 pi " 111111 ih i| m j| j । " r 11' i" 40 60 80 100120140160180200220240260280300320340360380400420 mmmm Abundance #49884: Benzophenone-2 4,5-tricarboxylic acid, trimethyl e 221 163 1T 38.40 38.60 38.80 39.00 39.20 5000 m/z 355.05 31.44% 356 325
76 103 135 - TTTTTTTTTTTTTTTTTTTTTT IETT 1P 1' '1111' I" 111 P',l P1 "P " 1P ” ' i mlz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #44359:2,6-Dimethyl-3,4-bis(trimethylsilyioxymethyi)pyridi 221 38.40 38.60 38.80 39.00 39.20 1 73 m/z 207.00 31.04% 5000 147 MWWWWAlMs 178 45 | I. I li _____ 296 CTTT —Tuu I it i"I | i i i i | < i ’ 11 i II 11 i 11 । 11' । 11 11 i 11 | । । । । । 11 n । i i u । i 11 i । TEEEI I I 1 1 1 1 f 1 ‘ J 1 1 m/z—> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 38.40 38.60 38.80 39.00 39.20
6423.D GCMS0408.M Wed Apr 10 12:23:12 2002 Page 2
NYC-WTC_000039689
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