GCMS surrogate recovery data for sample AE06423, April 2002

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APR0405\6423.D Vial: 9 Acq On 5 Apr 2002 7 :54 pm Operator: Sample gc/ms scan 3/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

40.58 0.73 ug/1 40940 Perylene-dl2 37.93

Hit# of 5 MW MolForm CAS# Qual

1 3,6-Dioxa-2,4,.5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 12 2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 10 3 4H-Pyrido[1,2-a]pyrimidine-3-carbox 221 C11H15N3O2 064399-29-7 9 4 Mercaptoacetic acid, bis (trimethyls 236 C8H20O2SSi2 006398-62-5 9 Abundance Scan 3871 (40.580 min): 6423. D (-) m/z 73.00 100.00%

0 73 147 221

5000 355 281 429 40.20 40.40 40.60 40.80 41.00 49 I 191 — --- m/z 221.05 76.45% T II T • "1 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #41682:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 221

73 5000 ' 1 i 1 40.20 40.40 40.60 40.80 41.00 191 m/z 147.05 72.92% 117 279 / I I | 1 . -------- — — mlz—> 50 100 150 200 250 300 350 400 450 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73 AMAAA W 207 40.20 40.40 40.60 40.80 41.00 5000 147 m/z 207.00 51.57% 34 103 281 | 395 wWuMW TIT 482 m/z—> 50 100 150 200 250 300 350 400 450 Abundance #27807: 4H-Pyrido[1,2-a]pyrimidine-3-carboxamide, 1,6,7,8-t TI TIT , I . T- , ! . , TIIEt i i , r- 221 40.20 40.40 40.60 40.80 41.00 m/z 355.05 40.81%

5000

I 1 109 135,162 188 1 — I t ill -1 I I 1 ' l ' ' TT 1//l*TTT1dI ' l ■ • ■ ■ i • । ■ > i 1 ■ ' > i T ■ ■ * i ■ m/z—> 50 100 150 200 250 300 350 400 450 40.20 40.40 40.60 40.80 41 00

6423 .D GCMS0408.M Wed Apr 10 12:23:13 2002 Page 3

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