GCMS analysis results, sample AE08210, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR1702\8210.D Vial: 21 Acq On : 18 Apr 2002 3:45 am Operator: Sample : gc/ms scan 4/8 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

40.47 0.59 ug/1 52910 Perylene-dl2 37.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,6-Dioxa-2,4,b,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 27 2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 12 3 Acetic acid, /[ (trimethylsilyl) oxy] - 220 C8H20O3S12 033581-77-0 10 4 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 10 Abundance Scan 3859 (40.475 min): 8210.D (-) m/z 73.00 100.00% 73 147 221 5000 281 355 f i i | i r i i । “ i i i i | i i > i-1 i ' i i i

429 40.20 40.40 40.60 40.80 193 m/z-> 1 i 50 1 ' 1.... ll ' ■ i 1 1 ' ■ i 1 100 150 200 —T r 250 , 253 1 327 ■ 300 ■ I" 1 1 350 i ' 400 1 ■ 1 i ' 41 .. 450 m/z 147.00 70.61% Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 2221

73 5000 / A AAM AAA M A, A/l 40.20 40.40 40.60 40.80 191 m/z 220.95 60.11% 117 279

m/z-> 1 1 I tk 1 1 1 1 50 100 U150 t ' i 1 200 ----------------- 250 300 350 400 450 Abundance #58871:1 -Monolinoleoylglycerol trimethylsilyl ether 73

40.20 40.40 40.60 40.80 207 5000 147 m/z 207.00 48.23% 34 103 281 395 I , 482 AroAo"oo ■ i 11 1 i 11 ‘ 1 1 ■ 1 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #27462: Acetic acid, ((trimethylsilyl)oxy)-, trimethylsilyl 73 40.20 40.40 40.60 40.80 147 m/z 281.00 29.06% 5000 aj/hot. 45 Li ‘dt 103 ' i' 1 177 205 , It m/z—> 50 100 150 200 250 300 350 400 450 40.20 40.40 40.60 40.80

8210.D GCMS0412.M Thu Apr 18 14:11:41 2002 Page 5

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