GCMS analysis results for sample AE06449, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \HPCHEM\ 1 \DATA\APR1 7026449.D Vial: 7 Acq On : 17 Apr 2002 2:06 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 16 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 37.32 0.87 ug/1 67619 Perylene-dl2 37.87 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,6-Dioxa-2,4,5,7-ttetrasilaoctane, 294 C10H3002Si4 004342-25-0 25 2 Trisiloxane, 1,1,1, 5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 16 3 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 13 4 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 12 Abundance Scan 3515 (37.317 min): 6449.D (-) m/ Z 73.00 100.00% 73

147 221 5000 281 355 429 40 , 327 37.00 37.20 37.40 37.60 — , ________ ill_______ a 193 ‘ I ' ' 1 ' l 1 ' 1 1 I 1 , 253, _ Al ’i ■ 11 l ll i 1 i 1 ■ - m/z 147.00 60.19% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #41682:3,6-Dioxa-2,4,5,7-tetrasiIaoctane, 2,2,4,4,5,5,7,7- 147 221

73 5000 A 37.00 37.20 37.40 37.60 191 m/z 221.05 59.64% 117 279 I I I i I ■ " i 1 ' m/z—> 50 100 150 200 250 300 350 400 450 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 A AAA A i 281 37.00 37.20 37.40 37.60 5000 m/z 281.00 38.87% __ 369 | 207 249 , ----- L— 338 ' i ■ m/z— > 50 100 150 200 250 350 300 400 450 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73 37.00 37.20 37.40 37.60 m/ z 355.05 37.81%| 207 5000 147 34 103 281 395 r l t —P ----- — ---------------- 1 ,. 482 ..AAA AN _ _______ ■ ■ J ■ ■ ■ 1 i ■ ■ ' 1 i ■ 1 1 1 i 1 ' 1 1 i m/z—> 50 - 100 150 200 250 300 350 400 450 37.00 37.20 37.40 37.60

6449.D GCMS0412.M Thu Apr 18 09:10:59 2002 Page 16

NYC-WTC_000039519